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Improved pharmacokinetics of AMG 517 through co-crystallization. Part 1: comparison of two acids with corresponding amide co-crystals.
Stanton, Mary K; Kelly, Ron C; Colletti, Adria; Kiang, Y-H; Langley, Meghan; Munson, Eric J; Peterson, Matthew L; Roberts, John; Wells, Mary.
Afiliación
  • Stanton MK; Amgen, Inc., 360 Binney Street, Cambridge, Massachusetts 02142, USA. mstanton@amgen.com
J Pharm Sci ; 99(9): 3769-78, 2010 Sep.
Article en En | MEDLINE | ID: mdl-20665842
The dissolution and pharmacokinetics (PK) of two carboxylic acid co-crystals (cinnamic acid and benzoic acid) with the corresponding amide co-crystals (cinnamamide and benzamide) of AMG 517 were investigated. Powder and intrinsic dissolution studies were performed in fasted simulated intestinal fluid (FaSIF). Suspension formulations in 1% polyvinylpyrrolidone K25 in water were administered orally at 100 mg/kg to rats. The four co-crystals were found to have faster intrinsic and powder dissolution rates in FaSIF than the free base. This correlated with a 2.4- to 7.1-fold increase in the area under the concentration-time curve in rat PK investigations. When contrasting the acid to its corresponding amide co-crystal, cinnamamide shows improvement over cinnamic acid, while benzamide and benzoic acid perform similarly.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Pirimidinas / Benzotiazoles / Canales Catiónicos TRPV Límite: Animals Idioma: En Revista: J Pharm Sci Año: 2010 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Pirimidinas / Benzotiazoles / Canales Catiónicos TRPV Límite: Animals Idioma: En Revista: J Pharm Sci Año: 2010 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos