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Chloro-substituted 3-alkylamino-4H-1,2,4-benzothiadiazine 1,1-dioxides as ATP-sensitive potassium channel activators: impact of the position of the chlorine atom on the aromatic ring on activity and tissue selectivity.
Pirotte, Bernard; de Tullio, Pascal; Nguyen, Quynh-Anh; Somers, Fabian; Fraikin, Pierre; Florence, Xavier; Wahl, Philip; Hansen, John Bondo; Lebrun, Philippe.
Afiliación
  • Pirotte B; Laboratoire de Chimie Pharmaceutique, Centre Interfacultaire de Recherche du Medicament (Drug Research Center), Universite de Liege, 1 Avenue de l'Hopital, B-4000 Liege, Belgium. B.Pirotte@ulg.ac.be
J Med Chem ; 53(1): 147-54, 2010 Jan 14.
Article en En | MEDLINE | ID: mdl-19919106
The synthesis of 5-chloro-, 6-chloro-, and 8-chloro-substituted 3-alkylamino/cycloalkylamino-4H-1,2,4-benzothiadiazine 1,1-dioxides is described. Their inhibitory effect on the insulin releasing process and their vasorelaxant activity was compared to that of previously reported 7-chloro-3-alkylamino/cycloalkylamino-4H-1,2,4-benzothiadiazine 1,1-dioxides. "5-Chloro" compounds were found to be essentially inactive on both the insulin-secreting and the smooth muscle cells. By contrast, "8-chloro" and "6-chloro" compounds were found to be active on insulin-secreting cells, with the "6-chloro" derivatives emerging as the most potent drugs. Moreover, the "6-chloro" analogues exhibited less myorelaxant activity than their "7-chloro" counterparts. 8-Chloro-3-isopropylamino-4H-1,2,4-benzothiadiazine 1,1-dioxide (25b) and 6-chloro-3-cyclobutylamino-4H-1,2,4-benzothiadiazine 1,1-dioxide (19e) were further identified as K(ATP) channel openers by radioisotopic measurements conducted on insulin-secreting cells. Likewise, current recordings on HEK293 cells expressing human SUR1/Kir6.2 channels confirmed the highly potent activity of 19e (EC(50) = 80 nM) on such types of K(ATP) channels. The present work indicates that 6-chloro-3-alkylamino/cycloalkylamino-4H-1,2,4-benzothiadiazine 1,1-dioxides appear to be more attractive than their previously described 7-chloro-substituted analogues as original drugs activating the SUR1/Kir6.2 K(ATP) channels.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Benzotiadiazinas / Canales de Potasio / Cloro / Islotes Pancreáticos / Óxidos S-Cíclicos / Diazóxido / Músculo Liso Vascular Tipo de estudio: Diagnostic_studies Límite: Animals / Humans Idioma: En Revista: J Med Chem Asunto de la revista: QUIMICA Año: 2010 Tipo del documento: Article País de afiliación: Bélgica Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Benzotiadiazinas / Canales de Potasio / Cloro / Islotes Pancreáticos / Óxidos S-Cíclicos / Diazóxido / Músculo Liso Vascular Tipo de estudio: Diagnostic_studies Límite: Animals / Humans Idioma: En Revista: J Med Chem Asunto de la revista: QUIMICA Año: 2010 Tipo del documento: Article País de afiliación: Bélgica Pais de publicación: Estados Unidos