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Interlaboratory comparison of methodologies for the measurement of urinary 8-oxo-7,8-dihydro-2'-deoxyguanosine.
Cooke, Marcus S; Barregard, Lars; Mistry, Vilas; Potdar, Neelam; Rozalski, Rafal; Gackowski, Daniel; Siomek, Agnieszka; Foksinski, Marek; Svoboda, Peter; Kasai, Hiroshi; Konje, Justin C; Sallsten, Gerd; Evans, Mark D; Olinski, Ryszard.
Afiliación
  • Cooke MS; Department of Cancer Studies and Molecular Medicine, Radiation and Oxidative Stress Section, University of Leicester, Leicester, UK. msc5@le.ac.uk
Biomarkers ; 14(2): 103-10, 2009 Mar.
Article en En | MEDLINE | ID: mdl-19330588
Urinary 8-oxo-7,8-dihydro-2'-deoxyguanosine (8-oxodGuo) is widely used as a marker of oxidative stress. Here we report the comparison of two, distinct chromatographic assays with an enzyme-linked immunosorbent assay (ELISA). The chromatographic assays displayed good agreement (r =:0.89, p < 0.0001), whereas there was markedly worse, albeit still significant, agreement with the ELISA (high-pressure liquid chromatography followed by gas chromatography (HPLC-GC/MS), r = 0.43; HPLC with electrochemical detection (HPLC-EC), r = 0.56; p < 0.0001). Mean values differed significantly between the chromatographic assays and the ELISA (HPLC-GC/MS 3.86, HPLC-EC 4.20, ELISA 18.70 ng mg(-1) creatinine; p < 0.0001). While it is reassuring to note good agreement between chromatographic assays, this study reveals significant short-comings in the ELISA, which brings into question its continued use in its present form.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Desoxiguanosina / Laboratorios Límite: Adult / Humans / Male / Middle aged Idioma: En Revista: Biomarkers Asunto de la revista: BIOQUIMICA Año: 2009 Tipo del documento: Article Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Desoxiguanosina / Laboratorios Límite: Adult / Humans / Male / Middle aged Idioma: En Revista: Biomarkers Asunto de la revista: BIOQUIMICA Año: 2009 Tipo del documento: Article Pais de publicación: Reino Unido