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Subphthalocyanine-fused dimers and trimers: synthetic, electrochemical, and theoretical studies.
Iglesias, Rodrigo S; Claessens, Christian G; Torres, Tomas; Herranz, M Angeles; Ferro, Victor R; de la Vega, Jose M García.
Afiliación
  • Iglesias RS; Departamento de Química Orgánica, Universidad Autónoma de Madrid, 28049-Madrid, Spain.
J Org Chem ; 72(8): 2967-77, 2007 Apr 13.
Article en En | MEDLINE | ID: mdl-17358079
Subphthalocyanine (SubPc)-fused dimers and trimers bearing fluorine, iodine, and thioether peripheral substituents were synthesized and characterized. Absorption spectroscopy and electrochemical studies revealed (i) that the substituents have a strong effect on the electronic properties of the macrocycles and (ii) that there is good communication between the subphthalocyaninic moieties within the oligomeric structures. Theoretical calculations at DFT/6-31G(d,p) computational level and electron density studies support the experimental findings. The frontier orbitals in the dimers and trimers were also shown to be significantly altered with respect to those of SubPcs as a consequence of the extension of the conjugation associated with symmetry breaking. Time-dependent density functional theory calculations reproduced the differences observed in the UV-vis spectra of the fused dimers and the monomeric SubPcs.
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Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: J Org Chem Año: 2007 Tipo del documento: Article País de afiliación: España Pais de publicación: Estados Unidos
Buscar en Google
Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: J Org Chem Año: 2007 Tipo del documento: Article País de afiliación: España Pais de publicación: Estados Unidos