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Determination of 234U/238U ratio: comparison of multi-collector ICPMS and ICP-QMS for water, hair and nails samples, and comparison with alpha-spectrometry for water samples.
Karpas, Z; Lorber, A; Sela, H; Paz-Tal, O; Hagag, Y; Kurttio, P; Salonen, L.
Afiliación
  • Karpas Z; Nuclear Research Center, Negev, P.O. Box 9001, Beer-Sheva 84190, Israel. karpas4@netvision.net.il
Radiat Prot Dosimetry ; 118(1): 106-10, 2006.
Article en En | MEDLINE | ID: mdl-15985497
The (234)U/(238)U ratio in water, hair and nails samples was determined by multi-collector inductively coupled plasma mass spectrometry (MC-ICPMS) and inductively coupled plasma quadrupole mass spectrometry (ICP-QMS) and by alpha-spectrometry for the water samples only. A correlation of 0.99 was found between the two ICPMS methods and of 0.98 with alpha-spectrometry. The range of activity ratios was between 0.9 and 2.6 according to the MC-ICPMS measurements. The reproducibility of both ICPMS techniques was better than 4% for water samples containing 1 mug l(-1) of uranium and a (234)U/(238)U atom ratio of 54.9 x 10(-6). Sample preparation for the ICPMS consisted of dilution of water samples containing >10 microg l(-1) of uranium and measurement time was approximately 1 min, while alpha-spectrometry involved pre-concentration and separation of the uranium and counting times of 1,000 min.
Asunto(s)
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Contaminantes Radiactivos del Agua / Abastecimiento de Agua / Monitoreo de Radiación / Uranio / Exposición a Riesgos Ambientales / Cabello / Uñas Tipo de estudio: Etiology_studies / Risk_factors_studies Límite: Humans Idioma: En Revista: Radiat Prot Dosimetry Año: 2006 Tipo del documento: Article País de afiliación: Israel Pais de publicación: Reino Unido
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Contaminantes Radiactivos del Agua / Abastecimiento de Agua / Monitoreo de Radiación / Uranio / Exposición a Riesgos Ambientales / Cabello / Uñas Tipo de estudio: Etiology_studies / Risk_factors_studies Límite: Humans Idioma: En Revista: Radiat Prot Dosimetry Año: 2006 Tipo del documento: Article País de afiliación: Israel Pais de publicación: Reino Unido