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Determination of isopropylmethylphenols in black seed oil by differential pulse voltammetry.
Michelitsch, Astrid; Rittmannsberger, Anna; Hüfner, Antje; Rückert, Ulla; Likussar, Werner.
Afiliación
  • Michelitsch A; Institut für Pharmazeutische Chemie und Pharmazeutische Technologie der Karl-Franzens-Universität Graz, Schubertstrasse 1, A-8010 Graz, Austria. astrid.ortner@kfunigraz.at
Phytochem Anal ; 15(5): 320-4, 2004.
Article en En | MEDLINE | ID: mdl-15508837
A differential pulse voltammetric method is presented for the determination of isopropylmethylphenols (carvacrol and/or thymol) in phytotherapeutic black seed oils. The voltammetric behaviours of these phenols were examined in various buffer systems over the pH range 3.5-10.0. In Sörensen buffered methanol solution (3:7; v:v; pH 8.5), the differential pulse voltammograms exhibited reproducible peaks at Ep + 0.49 V vs. silver-silver chloride-potassium chloride 3 M for both carvacrol and thymol. Under these conditions, a plot of peak height against concentration of the isopropylmethylphenols was found to be linear over the range 0.25-2.5 microg/mL (r = 0.999). The detection limit was 0.04 microg/mL. The described voltammetric method was tested on two black seed oils available on the Austrian market.
Asunto(s)
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Timol / Aceites de Plantas / Nigella sativa / Monoterpenos Idioma: En Revista: Phytochem Anal Asunto de la revista: BOTANICA / QUIMICA Año: 2004 Tipo del documento: Article País de afiliación: Austria Pais de publicación: Reino Unido
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Timol / Aceites de Plantas / Nigella sativa / Monoterpenos Idioma: En Revista: Phytochem Anal Asunto de la revista: BOTANICA / QUIMICA Año: 2004 Tipo del documento: Article País de afiliación: Austria Pais de publicación: Reino Unido