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Development of an ELISA for the detection of the residues of the fungicide iprovalicarb.
Lee, Jae Koo; Park, Sun Hwa; Lee, Eun Young; Kim, Yun Jung; Kyung, Kee Sung.
Afiliación
  • Lee JK; Department of Agricultural Chemistry, Chungbuk National University, Cheongju 361-763, Korea. jklee@cbnu.ac.kr
J Agric Food Chem ; 52(22): 6680-6, 2004 Nov 03.
Article en En | MEDLINE | ID: mdl-15506800
A competitive indirect enzyme-linked immunosorbent assay was developed for the fungicide iprovalicarb, using a polyclonal antibody produced against a hapten conjugated through the carboxyl group on the benzene ring to keyhole limpet hemocyanin. Under an optimized condition using a heterologous format, an IC(50) of 3.51 ng/mL and the lowest detection limit of 0.065 ng/mL were obtained. When the isopropoxy group was removed from the iprovalicarb structure for the synthesis of a hapten, the resulting hapten was not successful as an immunogen, indicating that the isopropyl moiety was an important epitope, as evidenced by the cross-reactivities of some structurally related compounds. When applied to the real crop and water samples, the recoveries were in the range of 80.52-144.70% (n = 4) and 72.11-100.43% (n = 4), respectively. Accordingly, this ELISA can be used as a useful method for monitoring iprovalicarb residues in crop and water samples.
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Valina / Ensayo de Inmunoadsorción Enzimática / Carbamatos / Residuos de Plaguicidas / Fungicidas Industriales Tipo de estudio: Diagnostic_studies Idioma: En Revista: J Agric Food Chem Año: 2004 Tipo del documento: Article Pais de publicación: Estados Unidos
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Valina / Ensayo de Inmunoadsorción Enzimática / Carbamatos / Residuos de Plaguicidas / Fungicidas Industriales Tipo de estudio: Diagnostic_studies Idioma: En Revista: J Agric Food Chem Año: 2004 Tipo del documento: Article Pais de publicación: Estados Unidos