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The effect of class-specific protease inhibitors on the stabilization of B-type natriuretic peptide in human plasma.
Belenky, Alexander; Smith, Andrew; Zhang, Bin; Lin, Spencer; Despres, Normand; Wu, Alan H B; Bluestein, Barry I.
Afiliación
  • Belenky A; Bayer Healthcare LLC, Diagnostics Division, Laboratory Testing Segment, Research and Development, 511 Benedict Avenue, Tarrytown, NY 10591, USA. alexander.belenky.b@bayer.com
Clin Chim Acta ; 340(1-2): 163-72, 2004 Feb.
Article en En | MEDLINE | ID: mdl-14734208
BACKGROUND: B-type natriuretic peptide (BNP) is a cardiac hormone that regulates hemodynamic equilibrium. In the circulation, its activity is controlled by proteolytic factors. Accurate measurement of BNP in a patient's plasma may be affected by degradation due to proteolysis. OBJECTIVE: We report on the identification and performance of classes of protease inhibitors that stabilize BNP in plasma. DESIGN AND METHODS: Using the Bayer ADVIA Centaur BNP assay, we measured the effect of arginine, serine and/or specific kallikrein protease inhibitors (PIs) on exogenous spiked or endogenous BNP in patient plasma. RESULTS: Compared to controls without inhibitor, all PIs were capable, to varying degrees, of retarding the rate of proteolytic degradation. The kallikrein-specific inhibitor, D-Phe-Phe-Arg-chloromethylketone (PPACK II) was most effective as a single constituent and was able to eliminate BNP degradation in patient samples for up to 6-10 days when stored at 2-8 degrees C. CONCLUSIONS: The stability of BNP was markedly increased in the presence of kallikrein-specific PPACK II and a broad spectrum of serine PIs. Use of these compounds offers a simple method of extending sample handling and storage of plasma samples containing BNP.
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Inhibidores de Proteasas / Péptido Natriurético Encefálico Tipo de estudio: Prognostic_studies Límite: Humans Idioma: En Revista: Clin Chim Acta Año: 2004 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Países Bajos
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Inhibidores de Proteasas / Péptido Natriurético Encefálico Tipo de estudio: Prognostic_studies Límite: Humans Idioma: En Revista: Clin Chim Acta Año: 2004 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Países Bajos