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Calcium binding properties of recombinant calcium binding protein 40, a major calcium binding protein of lower eukaryote Physarum polycephalum.
Nakamura, A; Okagaki, T; Takagi, T; Nakashima, K i; Yazawa, M; Kohama, K.
Afiliación
  • Nakamura A; Department of Pharmacology, Gunma University School of Medicine, Maebashi, Gunma 371-8511, Japan.
Biochemistry ; 39(13): 3827-34, 2000 Apr 04.
Article en En | MEDLINE | ID: mdl-10736183
Calcium binding protein 40 (CBP40) is a Ca(2+)-binding protein abundant in the plasmodia of Physarum polycephalum. CBP40 consists four EF-hand domains in the COOH-terminal half and a putative alpha-helix domain in the NH(2)-terminal half. We expressed recombinant proteins of CBP40 in Escherichia coli to investigate its Ca(2+)-binding properties. Recombinant proteins of CBP40 bound 4 mol of Ca(2+) with much higher affinity (pCa(1/2) = 6.5) than that of calmodulin. When residues 1-196 of the alpha-helix domain were deleted, the affinity for Ca(2+) decreased to pCa(1/2) = 4.6. A chimeric calmodulin was generated by conjugating the alpha-helix domain of CBP40 with calmodulin. The affinity of Ca(2+) for the chimeric calmodulin was higher than that for calmodulin, suggesting that the alpha-helix domain is responsible for the high affinity of CBP40 for Ca(2+). CBP40 forms large aggregates reversibly in a Ca(2+)-dependent manner. A mutant protein with a deletion of NH(2)-terminal 32 residues, however, could not aggregate, indicating the importance of these residues for the aggregation. The aggregation occurs above micromolar levels of Ca(2+) concentration, so it may only occur when CBP40 is secreted out of the plasmodial cells.
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Physarum / Proteínas Recombinantes de Fusión / Proteínas de Unión al Calcio / Proteínas Protozoarias Límite: Animals Idioma: En Revista: Biochemistry Año: 2000 Tipo del documento: Article País de afiliación: Japón Pais de publicación: Estados Unidos
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Physarum / Proteínas Recombinantes de Fusión / Proteínas de Unión al Calcio / Proteínas Protozoarias Límite: Animals Idioma: En Revista: Biochemistry Año: 2000 Tipo del documento: Article País de afiliación: Japón Pais de publicación: Estados Unidos