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Biological activity of synthesized 5-{1-[(4-chlorophenyl)sulfonyl]piperidin-4-yl}-2-mercapto-1, 3, 4-oxadiazole derivatives demonstrated by in silico and BSA binding studies
Iqbal, Javed; Rehman, Aziz-ur-; Abbasi, Muhammad Athar; Siddiqui, Sabahat Zahra; Rasool, Shahid; Ashraf, Muhammad; Iqbal, Ambar; Hamid, Sujhla; Chohan, Tahir Ali; Khalid, Hira; Laulloo, Sabina Jhaumeer; Shah, Syed Adnan Ali.
Afiliación
  • Iqbal, Javed; Government College University. Department of Chemistry. Lahore. PK
  • Rehman, Aziz-ur-; Government College University. Department of Chemistry. Lahore. PK
  • Abbasi, Muhammad Athar; Government College University. Department of Chemistry. Lahore. PK
  • Siddiqui, Sabahat Zahra; Government College University. Department of Chemistry. Lahore. PK
  • Rasool, Shahid; Government College University. Department of Chemistry. Lahore. PK
  • Ashraf, Muhammad; The Islamia University of Bahawalpur. Department of Chemistry. Bahawalpur. PK
  • Iqbal, Ambar; The Islamia University of Bahawalpur. Department of Chemistry. Bahawalpur. PK
  • Hamid, Sujhla; The Islamia University of Bahawalpur. Department of Chemistry. Bahawalpur. PK
  • Chohan, Tahir Ali; University of Veterinary and Animal Science. Institute of Pharmaceutical Science. Lahore. PK
  • Khalid, Hira; Forman Christian College University. Department of Chemistry. Lahore. PK
  • Laulloo, Sabina Jhaumeer; University of Mauritius. Department of Chemistry. Reduit. MU
  • Shah, Syed Adnan Ali; Universiti Teknologi MARA. Faculty of Pharmacy. Bandar Puncak Alam. MY
Braz. J. Pharm. Sci. (Online) ; 56: e18092, 2020. tab, graf
Article en En | LILACS | ID: biblio-1142491
Biblioteca responsable: BR40.1
Ubicación: BR40.1
ABSTRACT
We synthesized a series of compounds bearing pharmacologically important 1,3,4-oxadiazole and piperidine moieties. Spectral data analysis by 1H-NMR, 13C-NMR, IR and EI-MS was used to elucidate the structures of the synthesized molecules. Docking studies explained the different types of interaction of the compounds with amino acids, while bovine serum albumin (BSA) binding interactions showed their pharmacological effectiveness. Antibacterial screening of these compounds demonstrated moderate to strong activity against Salmonella typhi and Bacillus subtilis but only weak to moderate activity against the other three bacterial strains tested. Seven compounds were the most active members as acetyl cholinesterase inhibitors. All the compounds presented displayed strong inhibitory activity against urease. Compounds 7l, 7m, 7n, 7o, 7p, 7r, 7u, 7v, 7x and 7v were highly active, with respective IC50 values of 2.14±0.003, 0.63±0.001, 2.17±0.006, 1.13±0.003, 1.21±0.005, 6.28±0.003, 2.39±0.005, 2.15±0.002, 2.26±0.003 and 2.14±0.002 µM, compared to thiourea, used as the reference standard (IC50 = 21.25±0.15 µM). These new urease inhibitors could replace existing drugs after their evaluation in comprehensive in vivo studies.
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Texto completo: 1 Colección: 01-internacional Base de datos: LILACS Asunto principal: Simulación por Computador Idioma: En Revista: Braz. J. Pharm. Sci. (Online) Asunto de la revista: Farmacologia / Terapˆutica / Toxicologia Año: 2020 Tipo del documento: Article País de afiliación: Malasia / Mauricio / Pakistán Pais de publicación: Brasil

Texto completo: 1 Colección: 01-internacional Base de datos: LILACS Asunto principal: Simulación por Computador Idioma: En Revista: Braz. J. Pharm. Sci. (Online) Asunto de la revista: Farmacologia / Terapˆutica / Toxicologia Año: 2020 Tipo del documento: Article País de afiliación: Malasia / Mauricio / Pakistán Pais de publicación: Brasil