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1.
Food Res Int ; 177: 113836, 2024 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-38225113

RESUMO

An acidic beverage was formulated with xanthan gum (XG), pectin (P) and brewer spent grain (BSG) peptides with antioxidant and antihypertensive properties. The impact of hydrocolloids levels on peptide bioaccessibility was studied. Peptides were obtained from BSG using Purazyme and Flavourzyme enzymes. BSG peptides were fractionated by ultrafiltration (UF) and four fractions were obtained: F1 (>10 kDa), F2 (10-5 kDa), F3 (1-5 kDa), and F4 (<1 kDa). F3 showed the highest protein purity, ferulic acid content, proportion of amphipathic peptides, and bioactive properties (ABTS+ radical scavenging and ACE-I inhibitory activity). The identified peptides from F3 by tandem mass spectrometry were 138. In silico analysis showed that 26 identified peptides had ABTS+ inhibitory activity, while 59 ones presented good antihypertensive properties. The effect of XG and P levels on bioaccessibility of F3 peptides in the formulated beverages was studied by a central composite experimental design. It was observed that F3 peptides interacted with hydrocolloids by electrostatic forces at pH of formulated beverages. The addition of hydrocolloids to formulation modulated the release of the antioxidant peptides and protected the degradation of ACE-I inhibitory peptides from F3 during simulated gastrointestinal digestion. Finally, the level of hydrocolloids that produced intermediate viscosities in the formulated beverages improved the bioaccessibility of the F3 peptides.


Assuntos
Anti-Hipertensivos , Antioxidantes , Benzotiazóis , Polissacarídeos Bacterianos , Ácidos Sulfônicos , Anti-Hipertensivos/química , Antioxidantes/análise , Hidrólise , Inibidores da Enzima Conversora de Angiotensina/química , Pectinas/análise , Hidrolisados de Proteína/química , Peptídeos/química , Grão Comestível/química , Coloides/análise
2.
Foods ; 12(10)2023 May 22.
Artigo em Inglês | MEDLINE | ID: mdl-37238898

RESUMO

Aromatic plants represent about 0.7% of all medicinal plants. The most common are peppermint (main active ingredient: menthol) and chamomile (main active ingredient: luteolin), which are usually consumed in "tea bags" to make infusions or herbal teas. In this study, menthol and luteolin encapsulates using different hydrocolloids were obtained to replace the conventional preparation of these beverages. Encapsulation was carried out by feeding an infusion of peppermint and chamomile (83% aqueous phase = 75% water - 8% herbs in equal parts, and 17% dissolved solids = wall material in 2:1 ratio) into a spray dryer (180 °C-4 mL/min). A factorial experimental design was used to evaluate the effect of wall material on morphology (circularity and Feret's diameter) and texture properties of the powders using image analysis. Four formulations using different hydrocolloids were evaluated: (F1) maltodextrin-sodium caseinate (10 wt%), (F2) maltodextrin-soy protein (10 wt%), (F3) maltodextrin-sodium caseinate (15 wt%), and (F4) maltodextrin-soy protein (15 wt%). The moisture, solubility, bulk density, and bioavailability of menthol in the capsules were determined. The results showed that F1 and F2 presented the best combination of powder properties: higher circularity (0.927 ± 0.012, 0.926 ± 0.011), lower moisture (2.69 ± 0.53, 2.71 ± 0.21), adequate solubility (97.73 ± 0.76, 98.01 ± 0.50), and best texture properties. Those suggest the potential of these powders not only as an easy-to-consume and ecofriendly instant aromatic beverage but also as a functional one.

3.
Food Res Int ; 169: 112822, 2023 07.
Artigo em Inglês | MEDLINE | ID: mdl-37254398

RESUMO

The increase in the preference for vegan and vegetarian diets is directly related to changing eating habits and the need for plant-based alternatives to animal-based products, which are better for health, due to the high content of essential amino acids and lipid profile rich in polyunsaturated fatty acids, and have lower environmental impacts. In this scenario, there is a growing demand for plant-based foods, making it necessary to find new plant-based ingredients for application in foods and beverages. Flaxseed, chia seed, and Barbados gooseberry contain mucilage, a component with potential application in plant-based products. These hydrocolloids can be used as gelling agents, texture modifiers, stabilizers, and emulsifiers in solid and semi-solid foods. This review presents the extraction, characterization, and application of flaxseed, chia seed, and Barbados gooseberry mucilage for use in plant-based foods. It was found that mucilage composition varies due to the extraction method used, extraction conditions, and geographic location of the seed or leaf. However, applications in plant-based foods are currently limited, mainly focused on applying chia mucilage in bakery products and packaging. Research on applying flaxseed and Barbados gooseberry mucilage to plant-based products is limited, though it has been shown to have potential applications in packaging. Mucilage may also increase the nutritional profile of the product and provide better technological, functional, and sensory characteristics. Therefore, because of mucilage's excellent functional and technological properties, it is a promising candidate to act as an ingredient in plant-based food products.


Assuntos
Extratos Vegetais , Polissacarídeos , Polissacarídeos/análise , Extratos Vegetais/química , Sementes/química
4.
Polymers (Basel) ; 15(7)2023 Mar 27.
Artigo em Inglês | MEDLINE | ID: mdl-37050276

RESUMO

A polysaccharide was isolated from the exudate of a buriti tree trunk (Mauritia flexuosa). The molecular structure, thermal stability, morphology, crystallinity, and elemental composition of the product were investigated through spectroscopic techniques, such as Fourier-transform infrared spectroscopy (FTIR), nuclear magnetic resonance (NMR 1H and 13C), and energy-dispersive X-ray spectroscopy (EDS); thermogravimetric analysis (TG), differential scanning calorimetry (DSC), scanning electron microscopy (SEM), and X-ray diffraction (XRD). In addition to NMR molecular modeling studies, were performed to confirm the 1H and 13C chemical shifts to Gal and Xyl conformers. Buriti tree gum (BG) is an arabinogalactan, containing Rha, Ara, Xyl, and Gal, and degrades almost completely (98.5%) at 550 °C and has a maximum degradation peak at 291.97 °C, with a mass loss of 56.33%. In the temperature range of 255-290 °C, the energy involved in the BG degradation process was approximately 17 J/g. DSC indicated a glass transition temperature of 27.2 °C for BG, which had an irregular and heterogeneous morphology, with smooth or crumbling scaly regions, demonstrating the amorphous nature of BG that was confirmed by the XRD standard. EDS revealed the presence of carbon and oxygen, as well as calcium, magnesium, aluminum, silicon, chlorine, and potassium, in the BG composition.

5.
Gels ; 8(6)2022 Jun 06.
Artigo em Inglês | MEDLINE | ID: mdl-35735698

RESUMO

Background: Hydrocolloids are ingredients used to improve the technological properties of products; currently, there is a growing demand from the food industry and consumers to use natural ingredients and reduce the environmental impact. Methods: This work evaluated the effect of pH on hydrocolloid extraction from the pulp, seed, and peel of mango (Mangifera indica) var. hilaza and their chemical, physicochemical, techno-functional, and structural properties. Results: The main component of the hydrocolloid was the carbohydrates for pulp (22.59%) and peel (24.05%), and the protein for seed (21.48%) was corroborated by NIR spectra and associated with the technological and functional properties. The solubility increases with the temperature presenting values higher than 75% at 80 °C; the swelling index was higher than 30%, while the water holding capacity was higher in samples with higher carbohydrate content (110−121%). Moreover, a higher content of total phenolic compounds (21.61 ± 0.39−51.77 ± 2.48 mg GAE/g) and antioxidant activity (≥193.82 µMol Trolox/g) was obtained. The pH of extraction changes the color parameters and microstructural properties. Conclusions: Novel ingredients from mango pulp, seed, and peel at different pH levels have technological and functional properties that are potential use in the food industry as an alternative to the development of microstructural products.

6.
Gels ; 8(4)2022 Mar 30.
Artigo em Inglês | MEDLINE | ID: mdl-35448110

RESUMO

BACKGROUND: Natural ingredients have been employed to develop food products. METHODS: Hydrocolloids from butternut squash seeds (HBSSs) were extracted with water at pH 3, 7, and 10 and characterized bromatologically and rheologically; then these HBSSs were used to stabilize the dressing-type emulsion by evaluating its physicochemical, rheological, and microstructural properties. RESULTS: Hydrocolloids presented higher protein (from 20.43 to 39.39%) and carbohydrate (from 50.05 to 52.68%) content and rheological properties with a predominant elastic modulus. HBSSs extracted at pH 10 were used for the development of the dressing-type emulsion. The samples were stable during the storage period (15 days), with a good microstructural organization showing non-Newtonian fluid properties with shear-thinning behavior when the pseudoplasticity and the oil droplet size decreased with the addition of HBSS. CONCLUSIONS: Hydrocolloid constituents were detected surrounding the droplets of the emulsions, intensifying the effects of inner droplet interaction due to depletion events and a strong influence on the structure and physical stability. The hydrocolloids used to stabilize the dressing-type emulsions are additively promising in microstructured food design.

7.
São Paulo; s.n; s.n; 2022. 116 p. tab, tab.
Tese em Português | LILACS | ID: biblio-1396694

RESUMO

A fim de atender à demanda do público que atualmente busca por alimentos mais saudáveis, as indústrias têm procurado alternativas que possibilitem a aplicação de ingredientes que agreguem valor nutricional aos produtos. A redução de gorduras saturadas e trans em produtos alimentícios, bem como a inserção de cereais ou farinhas nutricionais, vem sendo aplicadas em produtos de panificação. Biscoitos recheados possuem como bases geralmente biscoitos à base de farinha de trigo. O objetivo foi desenvolver formulação de biscoitos recheados com substituição de gordura vegetal por organogel no recheio e de farinha de trigo por farinha de sorgo no biscoito, a fim de agregar valor nutricional ao produto. Foram desenvolvidos biscoitos recheados: 1) recheio controle e com substituição da gordura vegetal dos recheios por organogel elaborado com sistema emulsionado (colágeno + óleo vegetal + água), a fim de diminuir concentrações de gorduras saturadas e trans. 2) para a base elaborouse biscoitos controle (farinha de trigo) e com substituição parcial e total de farinha de trigo por farinha de sorgo em 50% (50FS) e 100% (100FS). Foram conduzidas nos recheios e das bases dos biscoitos análises físicas e físico-químicas (textura, atividade de água, cor, composição centesimal e reologia) para avaliação e para análise de estabilidade de 6 semanas. Os resultados apresentaram que o biscoito 50FS obteve melhor valor de textura (Controle: 16,09 ± 1,28 N; 50FS: 19,63 ± 5,68 N e 100FS: 10,09 ± 0,65 N) e menor teor de atividade de água (Semana 01: 0,327±0,01 e Semana 06: 0,389 ± 0,00) do que o biscoito controle, durante análise de estabilidade. O biscoito 100FS apresentou coloração mais avermelhada. Os biscoitos 50FS e 100FS apresentaram maior teor proteico do que o controle (Controle: 5,37 ± 0,23 %; 50FS: 5,64 ± 0,49 % e 100FS: 5,75 ± 0,49 %). O recheio com organogel apresentou maior dureza (N) durante análise de estabilidade do que o recheio controle (Semana 6 Organogel: 6,81±1,48; Controle: 4,29±0,38). Os parâmetros de adesividade, coesividade e gomosidade do recheio com organogel não apresentaram diferenças significativas (p > 0,05). Os valores de atividade de água da formulação com organogel foram mais altos do que o recheio controle (Semana 6 Organogel: 0,730±0,00; Controle: 0,555±0,01). O valor de L* foi maior para o recheio controle, apresentando coloração mais amarelada do que a formulação com organogel. O recheio com organogel apresentou redução de 65 % do teor lipídico e aumento do teor proteico. Os recheios controle, com organogel e de mercado apresentaram comportamento tixotrópico durante a avaliação reológica, sendo que o produto de mercado teve comportamento próximo à formulação controle, com recuperação quase total da estrutura. Foram desenvolvidos cinco produtos, sendo três inovadores com valor nutricional agregado, atendendo às legislações vigentes, vida útil mínima de 6 semanas e ao apelo do mercado atual, podendo ser comercializados como biscoito recheado


In order to satisfy the demand of the public that is currently looking for healthier foods industries have been looking for alternatives that allow the application of ingredients that add nutritional value to the products. The reduction of saturated and trans fats in food products, as well as the insertion of cereals or nutritional flours, has been applied in bakery products. Filled cookies are usually based on wheat flour. The objective was to develop a formulation of filled cookies with replacement of vegetable fat for organogel in the filling and wheat flour for sorghum flour in the biscuit, in order to add nutritional value to the product. In this study, cookies filled with vegetable fat and wheat flour were used as a control where: 1) filling was replaced by organogel elaborated with an emulsified system (collagen + vegetable oil + water); and 2) base was prepared with partial and total replacer of wheat flour for sorghum flour in 50% (50FS) and 100% (100FS). Physical and physicochemical analyzes (texture, water activity, color, proximate composition and rheology) were carried out on the fillings and bases of the biscuits for evaluation and for the stability analysis of 6 weeks. The results showed that the 50FS cookies had a better texture value (Control: 16,09±1,28 N; 50FS: 19,63±5,68N and 10,09±0,65 N) and lower content of water activity (Week 1: 0,327±0,01 and Week 6: 0,389±0,00) than the control cookie during stability analysis. The 100FS had a more reddish color. The 50FS and 100FS cookies had a higher protein content than the control (Control: 5,37±0,23 %; 50FS 5,64±0,49 %). The fillings with organogel showed a higher hardness (N) than the control during stability analysis (Week 6 Organogel: 6,81±1,48; Control: 4,29±0,38). The parameters of adhesiveness, cohesiveness and guminess of the filling with organogel showed no significant differences (p> 0.05). The water activity values of the organogel formulation were higher than the control filling (Week 6 Organogel: 0,730±0,00; Control: 0,555±0,01). The value of L * was higher for the control filling, showing a more yellowish color than the formulation with organogel. The filling with organogel showed a 65% reduction in lipid content and an increase in protein content. The control, organogel and market fillings showed a thixotropic behavior in the rheological evaluation, and the market product had a behavior close to the control formulation, with almost total recovery of the structure. Five products were developed, three of which were innovative with added nutritional value, in compliance with current legislation, a minimum shelf life of 6 weeks, which can be sold as a stuffed cookies.


Assuntos
Óleos de Plantas , Produção de Alimentos , Biscoitos , Gorduras/administração & dosagem , Reologia/instrumentação , Coloração e Rotulagem/instrumentação , Grão Comestível/efeitos adversos , Colágeno/efeitos adversos , Sorghum/classificação , Prazo de Validade de Produtos , Farinha/análise , Dureza , Indústrias/classificação , Valor Nutritivo
8.
J Dairy Res ; 88(3): 343-350, 2021 Aug.
Artigo em Inglês | MEDLINE | ID: mdl-34289915

RESUMO

The beneficial effects of a healthy diet on the quality of life have prompted the food industry to develop low-fat variants, but fat content directly affects the physicochemical and sensory properties of food products. The utilization of high-pressure homogenization (HP) and incorporation of hydrocolloids have been suggested as strategies to improve the physical stability and rheological properties of light cream. Thus, this study aims to analyze the associated effect of high-pressure homogenization (80 MPa) and three different hydrocolloids: microcrystalline cellulose, locust bean gum and xanthan gum, on emulsion stability and rheological properties of ultra-high-temperature (UHT) light cream (ULC) with a 15% w/w fat content. The stability of ULC was determined by the ζ potential of oil droplets and emulsion stability percentage. Rheological characterization was based on flow behavior tests and dynamic oscillatory measurements, which were carried out in a rheometer. Results showed that the high-pressure homogenization process did not influence the emulsion stability of the treatments. Moreover, the hydrocolloids added to systems present weak interactions with milk proteins since all ULC showed macroscopical phase separation. The samples presented the same rheological behavior and were classified as pseudoplastic fluids (n < 1). ULC treated at 80 MPa was significantly (P ≤ 0.05) more consistent than the treatments at 20 MPa. All ULC showed a predominant elastic behavior (G' > G″), and a remarkable increase in both G' and G″ at 80 MPa. The results presented in this study highlight the potential of HP for altering some rheological characteristics of UHT light cream, for example, to increase its consistency. These results are important for the dairy industry and ingredient suppliers, in the standardization of UHT light cream and/or to develop low-fat products.


Assuntos
Coloides/administração & dosagem , Laticínios , Gorduras na Dieta/análise , Manipulação de Alimentos/métodos , Temperatura Alta , Leite/química , Animais , Celulose , Fenômenos Químicos , Dieta com Restrição de Gorduras , Emulsões , Galactanos , Mananas , Gomas Vegetais , Polissacarídeos Bacterianos , Pressão , Reologia
9.
R. Inst. Adolfo Lutz ; 79: e1786, 30 set. 2020. tab
Artigo em Português | VETINDEX | ID: vti-32110

RESUMO

Com objetivo de produzir pão sem glúten com composição química aprimorada e boa qualidade sensorial, foram elaboradas três formulações com diferentes quantidades de mucilagem de quiabo: (F0) 0 mL; (F1) 100 mL; (F2) 150mL. Determinou-se: rendimento da mucilagem, composição centesimal, valor calórico e atributos sensoriais dos pães por meio de escala hedônica. A mucilagem aumentou o rendimento das F1 e F2. Não houve diferença no teor de proteínas e o teor de lipídios de 7,9 g 100 g-1 (F1) e 6,0 g 100 g-1 (F2) foram inferiores ao da F0. A umidade da F1 (32,15 g 100 g-1) foi menor que nas demais formulações, enquanto cinzas (0,70 g 100 g-1), carboidrato (56,75 g 100 g-1) e valor calórico (308,1 kcal 100 g-1) foram superiores. No teste sensorial, todos os atributos foram avaliados nas categorias “gostei ligeiramente” e “gostei extremamente” pela maioria dos julgadores. A F1 obteve avaliações superiores às da F2 para textura, cor e impressão global e não diferiu em nenhum dos atributos na F0. Conclui-se que a F1 pode ser uma opção viável na busca de pão sem glúten com composição química aprimorada, por conter menor teor de lipídio e umidade, maior teor de cinzas e boa aceitação sensorial.(AU)


With the goal of producing gluten-free bread with improved chemical composition and good sensorial quality, three formulations were prepared with different amounts of okra mucilage: (F0) 0 mL; (F1) 100 mL; (F2) 150 mL. From this was determined: mucilage yield, centesimal composition, caloric value and sensory attributes of bread by hedonic scale. Mucilage increased the yield of F1 and F2. There was no difference in protein content and the lipid content of 7.9 g 100 g-1 (F1) and 6.0 g 100 g-1 (F2) were lower than that of F0. The moisture content of F1 (32.15 g 100 g-1) was lower than the other formulations, while ash (0.70 g 100 g-1), carbohydrate (56.75 g 100 g-1) and caloric value (308,1 kcal 100 g-1) were higher. In the sensory test, attributes were rated in the categories “liked slightly” and “liked extremely” by most judges. F1 scored higher than F2 for texture, color and overall impression and did not differ in any of the attributes at F0. It can be concluded that F1 may be a viable option in the search for gluten-free bread with improved chemical composition, as it contains lower lipid and moisture content, higher ash content and good sensory acceptance.(AU)


Assuntos
Glutens/análise , Mucilagem Vegetal , Abelmoschus , Polissacarídeos , Pão/análise , Dieta Livre de Glúten , Doença Celíaca , Composição de Alimentos
10.
Food Chem ; 333: 127483, 2020 Dec 15.
Artigo em Inglês | MEDLINE | ID: mdl-32679415

RESUMO

The aim of the present paper was to unravel the effect of a standardized in vitro European protocol of digestion-fermentation over Ca(II)-alginate beads synthesized with sugars and biopolymers. Special emphasis on the antioxidant capacity using methods that simulate physiological conditions, short-chain fatty acids (SCFAs) production, and a detailed study of the microstructure of the gel network by SAXS at several scales (1-100 nm) were considered. Beads released high antioxidant capacity during digestion assessed by several methods, comparable to some common foods; antioxidant capacity was improved with sucrose and arabic gum inclusion in the formulation. After fermentation by gut microbiota, a ten-fold increase in the antioxidant values and an important SCFAs production were obtained, revealing the enhanced ability to produce these functional biomolecules. The microstructural analysis of Ca(II)-alginate showed an advantageous behavior: they slightly changed in oral and gastric fluids and partially dissolved their structure in intestinal fluid, where absorption occurs.


Assuntos
Alginatos/metabolismo , Antioxidantes/metabolismo , Ácidos Graxos Voláteis/biossíntese , Fermentação , Goma Arábica/química , Microesferas , Sacarose/química , Alginatos/química , Biomimética , Microbioma Gastrointestinal
11.
Acta Sci Pol Technol Aliment ; 19(1): 47-56, 2020.
Artigo em Inglês | MEDLINE | ID: mdl-32227697

RESUMO

BACKGROUND: Jamelão fruit (Syzygium cumini), has recently attracted interest as a functional food for being rich in anthocyanins, which has antioxidant power, attractive color and stability in high acid foods. METHODS: Samples of yoghurt with jamelão capsules obtained through the gelling process with sodium alginate solution and bioactive yoghurt (control + capsules) were evaluated. The samples were evaluated for composition, microbial viability, the stability on the anthocyanic pigments and its antioxidant activity. RESULTS: With the addition of jamelão pulp capsules there was a reduction in the Streptococcus thermophilus count. The addition of capsules in yoghurts were able to increase the amount of phenols and anthocyanins, as well as antioxidant potential at 28 days. The chromatographic analysis showed that process was efficient, being capable of encapsulating a large part of the bioactive compounds present in the pulp. CONCLUSIONS: The addition of jamelão pulp capsules to yoghurts was shown to be a promising and viable alternative, since the bioactive compounds present in the fruit were present in the yoghurt.


Assuntos
Syzygium/química , Iogurte/análise , Antocianinas/química , Antioxidantes/química , Frutas/química , Fenóis/química , Compostos Fitoquímicos , Streptococcus thermophilus/efeitos dos fármacos , Iogurte/microbiologia
12.
Rev. Inst. Adolfo Lutz (Online) ; 79: e1786, 31 mar. 2020. tab
Artigo em Português | LILACS, VETINDEX | ID: biblio-1489619

RESUMO

Com objetivo de produzir pão sem glúten com composição química aprimorada e boa qualidade sensorial, foram elaboradas três formulações com diferentes quantidades de mucilagem de quiabo: (F0) 0 mL; (F1) 100 mL; (F2) 150mL. Determinou-se: rendimento da mucilagem, composição centesimal, valor calórico e atributos sensoriais dos pães por meio de escala hedônica. A mucilagem aumentou o rendimento das F1 e F2. Não houve diferença no teor de proteínas e o teor de lipídios de 7,9 g 100 g-1 (F1) e 6,0 g 100 g-1 (F2) foram inferiores ao da F0. A umidade da F1 (32,15 g 100 g-1) foi menor que nas demais formulações, enquanto cinzas (0,70 g 100 g-1), carboidrato (56,75 g 100 g-1) e valor calórico (308,1 kcal 100 g-1) foram superiores. No teste sensorial, todos os atributos foram avaliados nas categorias “gostei ligeiramente” e “gostei extremamente” pela maioria dos julgadores. A F1 obteve avaliações superiores às da F2 para textura, cor e impressão global e não diferiu em nenhum dos atributos na F0. Conclui-se que a F1 pode ser uma opção viável na busca de pão sem glúten com composição química aprimorada, por conter menor teor de lipídio e umidade, maior teor de cinzas e boa aceitação sensorial.


With the goal of producing gluten-free bread with improved chemical composition and good sensorial quality, three formulations were prepared with different amounts of okra mucilage: (F0) 0 mL; (F1) 100 mL; (F2) 150 mL. From this was determined: mucilage yield, centesimal composition, caloric value and sensory attributes of bread by hedonic scale. Mucilage increased the yield of F1 and F2. There was no difference in protein content and the lipid content of 7.9 g 100 g-1 (F1) and 6.0 g 100 g-1 (F2) were lower than that of F0. The moisture content of F1 (32.15 g 100 g-1) was lower than the other formulations, while ash (0.70 g 100 g-1), carbohydrate (56.75 g 100 g-1) and caloric value (308,1 kcal 100 g-1) were higher. In the sensory test, attributes were rated in the categories “liked slightly” and “liked extremely” by most judges. F1 scored higher than F2 for texture, color and overall impression and did not differ in any of the attributes at F0. It can be concluded that F1 may be a viable option in the search for gluten-free bread with improved chemical composition, as it contains lower lipid and moisture content, higher ash content and good sensory acceptance.


Assuntos
Abelmoschus , Glutens/análise , Mucilagem Vegetal , Polissacarídeos , Pão/análise , Composição de Alimentos , Dieta Livre de Glúten , Doença Celíaca
13.
J Sci Food Agric ; 100(7): 3204-3211, 2020 May.
Artigo em Inglês | MEDLINE | ID: mdl-32105338

RESUMO

BACKGROUND: The incorporation of hydrocolloids into starch dispersions modifies their techno-functional properties, such as gelatinization, retrogradation, syneresis, and texture, among others. Their main function is to improve these properties and to promote greater stability of starch gels. Thus, the main objective of this study was to evaluate the effect of adding colloids (guar gum and xanthan gum) on the texture properties (hardness, elasticity, cohesiveness, and gumminess) and syneresis of the starch gels made from the common variety of arrowroot. Analysis of variance (ANOVA) and regression were carried out to analyze the effects of the treatments and variables with their respective interactions. RESULTS: The addition of guar gum and xanthan gum influenced the stability of the starch gels studied, and it was capable of reducing syneresis even at low concentrations, with a greater effect for xanthan gum. Both gums were capable of inhibiting syneresis at concentrations above 0.5%, throughout the storage time studied (5 days). The addition of these hydrocolloids was also shown to influence the following texture parameters: hardness, cohesiveness, and gumminess, but showed no effect on gel elasticity. CONCLUSION: The addition of hydrocolloids was shown to be an alternative way of increasing the stability and enhancing the textural properties of the starch gels in arrowroot. © 2020 Society of Chemical Industry.


Assuntos
Galactanos/química , Mananas/química , Marantaceae/química , Extratos Vegetais/química , Gomas Vegetais/química , Polissacarídeos Bacterianos/química , Amido/química , Coloides/química , Elasticidade , Géis/química , Dureza , Reologia
14.
J Food Sci Technol ; 56(7): 3264-3271, 2019 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-31274893

RESUMO

Lycopene extracted from pink grapefruit was encapsulated on Ca(II)-alginate beads with the addition of trehalose and galactomannans to improve its stability against freezing and drying. Three galactomannans of different physicochemical properties were studied since their inclusion affects both loading efficiency and release of lycopene in wet beads; however, there is no information about their performance during freezing and dehydration operations. The remaining lycopene and its stability towards isomerization were analyzed in beads subjected to continuous freezing, freezing/thawing cycles and vacuum- and freeze-drying. Isothermal crystallization studies were conducted by LF-NMR and related to beads formulation and lycopene stability. In the absence of excipients, lycopene was severely affected by all the treatments, retaining less than 20% of the original content. Alginate beads containing trehalose with guar gum protected more than 80% of the lycopene regardless of the employed freezing or drying methods. These beads concomitantly showed higher solid fraction than the other two galactomannans-containing systems, displaying guar gum ability to associate water. On the other hand, the addition of vinal gum affected lycopene stability (between 40 and 60% were recovered after treatments), even compromising the positive effect of a well-established cryoprotectant as trehalose. Thus, the addition of secondary excipients should be carefully conducted. The differences among galactomannans could be related to the substitution degree of the polymer chains, affecting the overall systems interactions. These results can contribute to excipients selection for the encapsulation of labile biomolecules in Ca(II)-alginate beads subjected to freezing and drying.

15.
J Prosthodont ; 28(8): 906-912, 2019 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-31350788

RESUMO

PURPOSE: To evaluate the antimicrobial activity and physico-mechanical properties of an irreversible hydrocolloid in which nanostructured silver vanadate decorated with silver nanoparticles (AgVO3 ) was added at various concentrations (0% - control, 2.5%, 5%, and 10% by weight). MATERIALS AND METHODS: The agar diffusion method (n = 10) was used to evaluate the inhibitory effect on the following species: Streptococcus mutans, Staphyloccocus aureus, Pseudomonas aeruginosa, Escherichia coli, and Candida albicans. The gelation time, flow capacity and plastic deformation were verified (n = 10). The data were analyzed using the Kruskal-Wallis test followed by the Dunn post-test, or via one-way ANOVA with multiple comparisons with a Bonferroni adjustment depending on the distribution (α = 0.05). RESULTS: All percentages of the nanomaterial were able to promote the antimicrobial activity of a hydrocolloid, with the formation of an inhibition zone (p < 0.05). In general, there was a dose-dependent effect on antimicrobial activity: higher concentrations of the nanomaterial promoted greater action except in the cases of P. aeruginosa (p < 0.001; F = 51.74) and S. aureus (p < 0.001), where the highest inhibition was for the 2.5% group. No difference was found in the gelation time when the control was compared with the groups with AgVO3 (p > 0.05). The difference was between the 5% and 10% groups (p = 0.007), and the latter promoted an increase in time. The flow capacity of the hydrocolloid with 5% of AgVO3 was significantly lower when compared with the control (p = 0.034). The AgVO3 influenced the plastic deformation (p < 0.001) in such a way that concentrations of 5% (p = 0.010) and 10% (p < 0.001) promoted an increase in this property when compared with the control. CONCLUSIONS: AgVO3 can be incorporated into an irreversible hydrocolloid as an antimicrobial agent without promoting adverse effects on physical-mechanical properties when used in concentrations of 2.5%.


Assuntos
Anti-Infecciosos , Nanopartículas Metálicas , Teste de Materiais , Prata , Staphylococcus aureus
16.
Dent J (Basel) ; 6(3)2018 Aug 02.
Artigo em Inglês | MEDLINE | ID: mdl-30072681

RESUMO

Irreversible hydrocolloids (IR) is a dental impression material commonly used in Brazilian and European dental practice because it is inexpensive, easy to handle, has good reproductive detail and is comfortable for the patient. This research aimed to analyze the chemical composition of eight different IRs for dental use. A sample of 0.2 g was weighed and transferred to a Teflon beaker moistened with drops of distilled or deionized water; 5 mL of nitric acid was added until total solubility of the sample; the solution was transferred to a 100 mL volumetric flask, the volume was filled with distilled or deionized water and homogenized. Thirty-five chemical elements were found: Lithium, Beryllium, Boron, Sodium, Magnesium, Aluminum, Silicon, Phosphorus, Potassium, Titanium, Manganese, Cobalt, Nickel, Vanadium, Zinc, Rubidium, Arsenic, Iron, Copper, Strontium, Yttrium, Zirconium, Niobium, Molybdenum, Ruthenium, Cadmium, Tin, Antimony, Barium, Lanthanum, Cerium, Mercury, Lead, Thorium and Uranium. Only one of the samples contained no Nickel, Antimony and Lead; and Arsenic and Uranium were found in 2 samples. This study provided evidence of high toxicity of the IR brands, pointing out the need for better quality control of this product, in order to prevent health damage in dentists, prosthesis technicians and patients.

17.
Semina Ci. agr. ; 36(3): 1317-1328, maio-jun. 2015. tab, graf
Artigo em Inglês | VETINDEX | ID: vti-28502

RESUMO

The removal of gluten results in many baking problems and many gluten-free products currently available in the market are of low quality. The addition of hydrocolloids, however, is an option to improve technological characteristics. The objective of this study was to evaluate the influence of the addition of methylcellulose and xanthan gum on the technological characteristics of gluten-free cakes made with 100% rice flour. Cakes using hydrocolloids at different concentrations were developed through an experimental design that evaluated technological features such as specific volume, crumb hardness and overall quality score. Mathematical models were obtained to describe the hardness and the score of cakes as a function of the addition of xanthan and methylcellulose. The smallest value of crumb hardness of the cakes was obtained when concentrations of 0.4% xanthan and 2% methylcellulose were added. With regards to the score, the highest value was obtained with the lowest levels of hydrocolloids, whose formulation contained 0.2% xanthan gum and 1% methylcellulose. It can be concluded that the addition of xanthan gum and methylcellulose enabled the development of a gluten-free cake with a softer crumb that presents technological quality attributes similar to that of a wheat cake.(AU)


A remoção do glúten resulta em problemas para a panificação e muitos dos produtos sem glúten disponíveis no mercado são de baixa qualidade, contudo a adição de hidrocolóides é uma opção para melhorar suas características tecnológicas. Este trabalho teve como objetivo avaliar a influência da adição de metilcelulose e goma xantana nas características tecnológicas de bolos sem glúten elaborados com 100% de farinha de arroz. Foram elaborados bolos utilizando hidrocolóides em diferentes concentrações através de planejamento experimental, sendo avaliadas características tecnológicas como volume específico, dureza do miolo e pontuação total. Foram obtidos modelos matemáticos para descrever a dureza e a pontuação dos bolos, em função da adição de xantana e metilcelulose. O menor valor de dureza do miolo dos bolos foi obtido quando adicionadas as concentrações de 0,4% de xantana e 2% de metilcelulose. Em relação a pontuação, o maior valor foi obtido com os menores teores dos hidrocolóides, cuja formulação continha 0,2% de goma xantana e 1% de metilcelulose. Pode-se concluir que a adição de goma xantana e metilcelulose proporcionou o desenvolvimento de um bolo sem glúten com miolo mais macio e apresentando atributos de qualidade tecnológica semelhantes a um bolo de trigo.(AU)


Assuntos
Dieta Livre de Glúten , Metilcelulose
18.
Semina ciênc. agrar ; 36(3): 1317-1328, 2015. tab, graf
Artigo em Inglês | VETINDEX | ID: biblio-1499977

RESUMO

The removal of gluten results in many baking problems and many gluten-free products currently available in the market are of low quality. The addition of hydrocolloids, however, is an option to improve technological characteristics. The objective of this study was to evaluate the influence of the addition of methylcellulose and xanthan gum on the technological characteristics of gluten-free cakes made with 100% rice flour. Cakes using hydrocolloids at different concentrations were developed through an experimental design that evaluated technological features such as specific volume, crumb hardness and overall quality score. Mathematical models were obtained to describe the hardness and the score of cakes as a function of the addition of xanthan and methylcellulose. The smallest value of crumb hardness of the cakes was obtained when concentrations of 0.4% xanthan and 2% methylcellulose were added. With regards to the score, the highest value was obtained with the lowest levels of hydrocolloids, whose formulation contained 0.2% xanthan gum and 1% methylcellulose. It can be concluded that the addition of xanthan gum and methylcellulose enabled the development of a gluten-free cake with a softer crumb that presents technological quality attributes similar to that of a wheat cake.


A remoção do glúten resulta em problemas para a panificação e muitos dos produtos sem glúten disponíveis no mercado são de baixa qualidade, contudo a adição de hidrocolóides é uma opção para melhorar suas características tecnológicas. Este trabalho teve como objetivo avaliar a influência da adição de metilcelulose e goma xantana nas características tecnológicas de bolos sem glúten elaborados com 100% de farinha de arroz. Foram elaborados bolos utilizando hidrocolóides em diferentes concentrações através de planejamento experimental, sendo avaliadas características tecnológicas como volume específico, dureza do miolo e pontuação total. Foram obtidos modelos matemáticos para descrever a dureza e a pontuação dos bolos, em função da adição de xantana e metilcelulose. O menor valor de dureza do miolo dos bolos foi obtido quando adicionadas as concentrações de 0,4% de xantana e 2% de metilcelulose. Em relação a pontuação, o maior valor foi obtido com os menores teores dos hidrocolóides, cuja formulação continha 0,2% de goma xantana e 1% de metilcelulose. Pode-se concluir que a adição de goma xantana e metilcelulose proporcionou o desenvolvimento de um bolo sem glúten com miolo mais macio e apresentando atributos de qualidade tecnológica semelhantes a um bolo de trigo.


Assuntos
Dieta Livre de Glúten , Metilcelulose
19.
Braz. arch. biol. technol ; Braz. arch. biol. technol;56(2): 311-318, Mar.-Apr. 2013. graf, tab
Artigo em Inglês | LILACS | ID: lil-675650

RESUMO

The objective of this work was to evaluate the application of carrageenan (CAR) to improve the functional properties of the jerked beef (JF) and to increase its processing yield. JB produced from Vastus lateralis with CAR (1.0%) at 25ºC and NaCl (15.0%) had approximately 15.0% higher moisture and a 32.0% higher processing yield in comparison to the control samples.JB-CAR presented shear force approximately 5.0 and 20% lower in the samples uncooked salted and desalted cooked, respectively, and sensorial acceptance above 80%. The results demonstrated the possibility of applying carrageenan to jerked beef in order to obtain an increase in the processing yield and a tender product while maintaining the sensorial quality and its intermediate-moisture meat product nature.

20.
Semina ciênc. agrar ; 34(1): 209-226, 2013.
Artigo em Português | LILACS-Express | VETINDEX | ID: biblio-1499109

RESUMO

This study was conducted to evaluate the physical-chemical, sensory and microbiological characteristics of fermented dairy beverages prepared with 10% sucrose, 50% milk and 50% whey and added five different stabilizers/thickeners in two concentrations (0,50% and 1,00% in relation to the final formulation). Ten treatments have been developed: PCPS 1,00% = protein (0,50%) and whey protein concentrate (0,50%); GP 1,00% = powdered gelatin (1,00%); GG 1,00% = guar gum (1,00%); AM 1.00% = corn starch (1,00%); GGCMC 1,00% = guar gum (0,50%) and carboxymethylcellulose (0,50%); PCPS 0,50 % = protein (0,25%) and whey protein concentrate (0,25%); GP 0.50% = powdered gelatin (0,50%); GG 0.50% = guar (0,50%); AM 0,50% = corn starch (0,50%); GGCMC 0,50% = guar gum (0,25%) and carboxymethylcellulose (0,25%). The fermented dairy beverages were evaluated for pH, acidity in lactic acid, moisture, ash, fat, protein, viscosity, syneresis, sensory acceptance (in a nine-point hedonic scale) and count of coliforms at 35ºC and 45C. The results were submitted to ANOVA and mean test with significance level of 5%. It was observed that the types and percentages of stabilizers/thickeners mainly influenced the values of syneresis, viscosity and acceptance of samples. Those of the treatments containing protein and whey protein concentrate (1,00%), guar gum (1,00%) and gelatin (0,50%) showed viscosity/consis


Este trabalho foi realizado com o objetivo de avaliar as características físico-químicas, sensoriais e a qualidade microbiológica de bebidas lácteas fermentadas elaboradas com 10% de sacarose, 50% de leite e 50% de soro de queijo e adicionadas de cinco diferentes estabilizantes/espessantes em duas concentrações (0,50% e 1,00% em relação à formulação final), propondo uma formulação com boa aceitação. Foram desenvolvidos dez tratamentos: PCPS 1,00% = proteína (0,50%) e concentrado proteico de soro (0,50%); GP 1,00% = gelatina em pó (1,00%); GG 1,00% = goma guar (1,00%); AM 1,00% = amido de milho (1,00%); GGCMC 1,00% = goma guar (0,50%) e carboximetilcelulose (0,50%); PCPS 0,50% = proteína (0,25%) e concentrado proteico de soro (0,25%); GP 0,50% = gelatina em pó (0,50%); GG 0,50% = goma guar (0,50%); AM 0,50% = amido de milho (0,50%); GGCMC 0,50% = goma guar (0,25%) e carboximetilcelulose (0,25%). As bebidas lácteas fermentadas foram avaliadas quanto ao pH, acidez em ácido lático, umidade, cinzas, lipídios, proteína, viscosidade, sinérese, aceitação sensorial (escala hedônica de nove pontos) e contagem de coliformes a 35ºC e 45C. Os resultados obtidos, submetidos a ANOVA e teste de médias (nível de significância a 5%), revelaram que os tipos e as porcentagens dos estabilizantes/espessantes influenciaram principalmente os valores de sinérese, viscosidade e aceitação das amostras.

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