RESUMO
In this work, we report on the solid-state reaction synthesis of SrZrO3 phosphors, and their beta particle irradiation excited thermoluminescence (TL) characterization. X-ray diffraction data confirmed the obtention of the orthorhombic phase of SrZrO3. Through computational glow curve deconvolution, the whole glow curve was resolved into six individual first order kinetics peaks. This is the first report concerning the usefulness of SrZrO3 as TL dosimeter. The synthesized phosphors exhibit TL emission from below 100 °C up to above 300 °C, being the most intense TL between 200 and 300 °C, as well as a remarkable reproducibility of the TL response in repeated irradiation-TL readout cycles.
RESUMO
In this work, the synthesis of SrB4O7 through solid state reaction and its beta particle excited thermoluminescence (TL) are reported. The glow curves show maxima around 200 and 300 -considered suitable for TL dosimetry-, and a remarkable reproducibility in successive irradiation - TL readout cycles. The integrated TL exhibits a linear dependence upon the irradiation dose in the tested dose range (from 1.0 up to 8.0 Gy). The lower detection limit and the sensitivity relative to the TLD-100 dosimeter are 88 mGy and 0.49, respectively. From the results here presented, we conclude that SrB4O7 synthesized through solid state reaction can be considered a phosphor material interesting to develop TL dosimeters.
RESUMO
The synthesis and thermoluminescence (TL) characterization of self-agglomerating pellet-shaped CaSO4 phosphors, through a low cost and environmentally friendly method is reported. In order to investigate their TL features, some samples were exposed to beta particle irradiation in the dose range from 0.07 to 10â¯Gy. Characteristic TL glow curve consists of a single main maximum located at 216⯰C, which is considered stable, hence, suitable for dosimetry applications. The dose-response was remarkable linear. Moreover, the lower detection limit was determined to be 6.0⯵Gy, and the relative TL sensitivity twice the one from the commercial TLD-100 dosimeter.