RESUMO
It is possible to apply the k(0)-method using a simplified equation for concentration calculations using Excel spreadsheet, using comparators without making corrections. The objective of this study was to confirm that the k(0)-standardization method is more efficient and accurate than this "k(0)-comparator" procedure, applying suitable software that takes into account several corrections. The reference material GBW07401 soil was analyzed in this study. Relative Bias and u-score tests were used in order to evaluate the overall results.
RESUMO
In this work, a comparative study of neutron activation analysis (NAA) was performed by the nuclear institutes: CDTN/CNEN-Brazil, CCHEN-Chile and the SCK.CEN-Belgium aiming to investigate some generic, manipulated and reference medicines largely commercialized in Brazil. Some impurities such as: As, Ba, Br, Ce, Co, Cr, Eu, Fe, Hf, Sb, Sc, Sm, Ti and Zn were found, and the heterogeneity of the samples pointed out the lack of an efficient public system of quality control.