RESUMO

Complete assignment of (1)H and (13)C NMR chemical shifts and J((1)H/(1)H and (1)H/(19)F) coupling constants for 22 1-phenyl-1H-pyrazoles' derivates were performed using the concerted application of (1)H 1D and (1)H, (13)C 2D gs-HSQC and gs-HMBC experiments. All 1-phenyl-1H-pyrazoles' derivatives were synthesized as described by Finar and co-workers. The formylated 1-phenyl-1H-pyrazoles' derivatives were performed under Duff's conditions.

Assuntos

Fenóis/química , Prótons , Pirazóis/química , Isótopos de Carbono , Estrutura Molecular , Ressonância Magnética Nuclear Biomolecular , Fenóis/síntese química , Pirazóis/síntese química , Padrões de Referência