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Colloids Surf B Biointerfaces ; 180: 141-149, 2019 Aug 01.
Artigo em Inglês | MEDLINE | ID: mdl-31039515

RESUMO

The synthesis and applications of anisotropic nanostructures have attracted much attention in the last decade. The nanoflower-type structures are one of the nanomaterials with anisotropic structures most investigated because of owing to high densities of edges, corners, and stepped atoms present on their nano-petals. Here, silver nanoparticles obtained by a one-step green synthesis method using extract from Kalanchoe Daigremontiana´s leaves are reported. To identify the compounds responsible for reduction of silver ions, the functional groups present in plant extract were investigated by UV-vis and FTIR. Ag nanoparticles were characterized by UV-vis, XPS, ζ-potential, XRD, and SEM-EDS. Different solvents were used to eliminate agglomeration of the silver nanoparticles. These solvents produced nanoflower-like morphology with abundant nano-petals. This is the first report of the synthesis of Ag nanoflowers formed by green synthesis method using Kalanchoe Daigremontiana extract. The synthesized Ag nanoflowers are faced center cubic structure in nature with a petal thickness approximately of 25 nm. Photocatalytic activity of the different Ag nanostructures was evaluated through the degradation of methylene blue, where the degradation time as low as 1 min is reported. Furthermore these green synthesized Ag nanoflowers were found to show high antibacterial activity against Gram-negative bacteria Escherichia coli and Gram-positive Staphylococcus aureus.


Assuntos
Antibacterianos/química , Química Verde , Kalanchoe/química , Nanopartículas Metálicas/química , Nanoestruturas/química , Prata/química , Anisotropia , Antibacterianos/farmacologia , Catálise , Escherichia coli/efeitos dos fármacos , Escherichia coli/crescimento & desenvolvimento , Nanopartículas Metálicas/ultraestrutura , Azul de Metileno/química , Nanoestruturas/ultraestrutura , Oxirredução , Tamanho da Partícula , Processos Fotoquímicos , Extratos Vegetais/química , Folhas de Planta/química , Prata/farmacologia , Staphylococcus aureus/efeitos dos fármacos , Staphylococcus aureus/crescimento & desenvolvimento
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