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Eur J Pharm Biopharm ; 55(3): 313-21, 2003 May.
Artículo en Inglés | MEDLINE | ID: mdl-12754006

RESUMEN

The present study was conducted in order to analyze the viability of the spouted bed process for application of a gastric-resistant coating to soft gelatin capsules. The variables investigated were: included angle of conical base, (gamma), the relation between the feed mass flow rate of the coating suspension and the feed mass flow rate of spouting gas (W(s)/W(g)); the ratio between the flow rate of the spouting gas and the flow rate at minimum spouting condition (Q/Q(ms)); the mass of capsules in the bed (M(0)), and the capsule's size. The product quality was measured by disintegration tests, traction x deformation tests, image analysis and by the evaluation of the coating mass distribution and shape factor variation during the coating operation. The experiments were performed in a spouted bed with a column diameter of 200 mm and included a conical base angle of 40 degrees. The best coating efficiency values were obtained for M(0)=300 g. Coating efficiency tended to increase with increasing W(s)/W(g) ratio. Disintegration tests showed that the gastric-resistant effect was obtained with a coating mass of 3.86 mg/cm(2). The shape factor increase during the coating operation. The capsule's coating mass distribution tended to maintain the original distribution.


Asunto(s)
Cápsulas/normas , Gelatina/normas , Comprimidos Recubiertos/normas , Tecnología Farmacéutica/normas , Cápsulas/síntesis química , Gelatina/síntesis química , Comprimidos Recubiertos/síntesis química , Tecnología Farmacéutica/instrumentación , Tecnología Farmacéutica/métodos
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