RESUMEN

OBJECTIVE: This study aims to evaluate the influence of different air-abrasion pressures and subsequent heat treatment on the flexural strength, surface roughness, and crystallographic phases of highly translucent partially stabilized zirconia (Y-PSZ), and on the tensile bond strength of resin cement to Y-PSZ. METHODOLOGY: Fully sintered zirconia specimens were ground with SiC paper (control) and/or air-abraded with 50 µm particles of alumina at 0.1, 0.15, 0.2, or 0.3 MPa or left as-sintered. After air-abrasion at 0.2 MPa (0.2AB), additional specimens were then heated to 1500°C, and held for one hour at this temperature (0.2AB+HT1h). Flexural strength and surface roughness were evaluated. Crystalline phase identification was also carried out using X-ray diffraction. Bonded zirconia specimens with self-adhesive resin cement were stored in distilled water at 37°C for 24 h, either with or without aging (thermal cycling 4-60°C/20000). Results were analyzed statistically by ANOVA and Tukey-Kramer tests. RESULTS: The flexural strength decreased with the increase in air-abrasion pressure, while in contrast, the surface roughness increased. The lowest flexural strength and the highest roughness value were found for the 0.2AB and 0.3AB groups, respectively. All groups contained cubic-, tetragonal ( t )-, and rhombohedral ( r )-ZrO2 phases with the exception of the as-sintered group. Upon increasing the air-abrasion pressure, the relative amount of the r -ZrO2 phase increased, with a significant amount of r -ZrO2 phase being detected for the 0.2AB and 0.3AB groups. The 0.2AB+HT1h group exhibited a similar flexural strength and t -ZrO2 phase content as the as-sintered group. However, the 0.2AB group showed a significantly higher tensile bond strength (p<0.05) than the 0.2AB+HT1h group before and after aging. CONCLUSION: Micromechanical retention by alumina air-abrasion at 0.2 MPa, in combination with chemical bonding of a resin to highly translucent Y-PSZ using a MDP-containing resin cement may enable durable bonding.

Asunto(s)

Abrasión Dental por Aire/métodos , Óxido de Aluminio/química , Recubrimiento Dental Adhesivo/métodos , Cementos de Resina/química , Circonio/química , Análisis de Varianza , Resistencia Flexional , Calor , Ensayo de Materiales , Microscopía Confocal/métodos , Valores de Referencia , Reproducibilidad de los Resultados , Propiedades de Superficie , Resistencia a la Tracción , Difracción de Rayos X/métodos

RESUMEN

Abstract Objective This study aims to evaluate the influence of different air-abrasion pressures and subsequent heat treatment on the flexural strength, surface roughness, and crystallographic phases of highly translucent partially stabilized zirconia (Y-PSZ), and on the tensile bond strength of resin cement to Y-PSZ. Methodology Fully sintered zirconia specimens were ground with SiC paper (control) and/or air-abraded with 50 µm particles of alumina at 0.1, 0.15, 0.2, or 0.3 MPa or left as-sintered. After air-abrasion at 0.2 MPa (0.2AB), additional specimens were then heated to 1500°C, and held for one hour at this temperature (0.2AB+HT1h). Flexural strength and surface roughness were evaluated. Crystalline phase identification was also carried out using X-ray diffraction. Bonded zirconia specimens with self-adhesive resin cement were stored in distilled water at 37°C for 24 h, either with or without aging (thermal cycling 4-60°C/20000). Results were analyzed statistically by ANOVA and Tukey-Kramer tests. Results The flexural strength decreased with the increase in air-abrasion pressure, while in contrast, the surface roughness increased. The lowest flexural strength and the highest roughness value were found for the 0.2AB and 0.3AB groups, respectively. All groups contained cubic-, tetragonal ( t )-, and rhombohedral ( r )-ZrO2 phases with the exception of the as-sintered group. Upon increasing the air-abrasion pressure, the relative amount of the r -ZrO2 phase increased, with a significant amount of r -ZrO2 phase being detected for the 0.2AB and 0.3AB groups. The 0.2AB+HT1h group exhibited a similar flexural strength and t -ZrO2 phase content as the as-sintered group. However, the 0.2AB group showed a significantly higher tensile bond strength (p<0.05) than the 0.2AB+HT1h group before and after aging. Conclusion Micromechanical retention by alumina air-abrasion at 0.2 MPa, in combination with chemical bonding of a resin to highly translucent Y-PSZ using a MDP-containing resin cement may enable durable bonding.

Asunto(s)

Circonio/química , Recubrimiento Dental Adhesivo/métodos , Cementos de Resina/química , Abrasión Dental por Aire/métodos , Óxido de Aluminio/química , Valores de Referencia , Propiedades de Superficie , Resistencia a la Tracción , Difracción de Rayos X/métodos , Ensayo de Materiales , Reproducibilidad de los Resultados , Análisis de Varianza , Microscopía Confocal/métodos , Resistencia Flexional , Calor

RESUMEN

PURPOSE: To evaluate the influence of particle and air-abrasion on the surface characterization and shear bond strength (SBS) of a Y-TZP ceramic with a resin cement. MATERIALS AND METHODS: Y-TZP specimens were air-abraded with 50 µm alumina particles; 120 µm alumina particles; 30 µm silica-coated alumina particles (Rocatec Soft); 110 µm silica-coated alumina particles (Rocatec Plus). Air-abrasion was performed before (BS); after (AS); before and after (BAS) zirconia sintering. Surface characterization included roughness (n = 10), wettability (n = 10), morphology (n = 2), and elemental composition (n = 2). For SBS (n = 11), composite resin discs were bonded to the air-abraded and silane-treated zirconia surface, with the resin cement RelyX ARC. Failure mode was determined. Roughness, wettability, and SBS data were analyzed by two-way ANOVA with pairwise interaction and Tukey's test (α = 0.05). RESULTS: Air-abrasion performed with coarser particles at BS and BAS moments provided the highest roughness values, while the lowest roughness values were observed with particles combined with AS moment (p < 0.01). Rocatec Plus provided lower contact angle than the 120 µm alumina particles (p = 0.013), and BAS exhibited lower contact angle than BS (p = 0.002). The combinations 120 µm/BS and the silica-coated alumina particles/AS and /BAS showed the highest SBS (p < 0.05). The combination of each particle/BAS was statistically similar to the same particle/AS. Failure mode was 100% adhesive for all groups. The interaction particle size/air-abrasion moment determined the morphological pattern. Silicon was observed only in the Rocatec groups. CONCLUSIONS: Roughness was influenced by the particle size and was higher when the zirconia was air-abraded in its green stage. The particle composition played an important role in the wettability and both studied air-abrasion moments provided similar wettability than the one in which air-abrasion is usually performed. The highest SBS values were observed in the three moments, by using certain particles for each moment.

Asunto(s)

Abrasión Dental por Aire/métodos , Cementos de Resina/química , Resistencia al Corte , Itrio/química , Circonio/química , Óxido de Aluminio/química , Análisis de Varianza , Bisfenol A Glicidil Metacrilato , Resinas Compuestas/química , Recubrimiento Dental Adhesivo , Cementos Dentales , Materiales Dentales/química , Fracaso de la Restauración Dental , Análisis del Estrés Dental , Humanos , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Tamaño de la Partícula , Polietilenglicoles , Ácidos Polimetacrílicos , Dióxido de Silicio/química , Propiedades de Superficie , Humectabilidad

RESUMEN

OBJECTIVES: To evaluate the effects of dentin pretreatment and temperature on the bond strength of a universal adhesive system to dentin. MATERIAL AND METHODS: Ninety-six extracted non-carious human third molars were randomly divided into 12 groups (n=8) according to Scotchbond Universal Adhesive (SbU) applied in self-etch (SE) and etch-and-rinse (ER) mode, adhesive temperature (20°C or 37°C) and sodium bicarbonate or aluminum oxide air abrasion. After composite build up, bonded sticks with cross-sectional area of 1 mm2 were obtained to evaluate the microtensile bond strength (µTBS). The specimens were tested at a crosshead speed of 0.5 mm/min on a testing machine until failure. Fractured specimens were analyzed under stereomicroscope to determine the failure patterns in adhesive, cohesive (dentin or resin) and mixed fractures. The microtensile bond strength data was analyzed using two-way ANOVA and Tukey's test (α=5%). RESULTS: Interaction between treatment and temperature was statistically significant for SbU applied in self-etch technique. Both dentin treatments showed higher bond strength for ER mode, regardless of adhesive temperature. When compared to control group, sodium bicarbonate increased bond strength of SbU in SE technique. Adhesive temperature did not significantly affect the µTBS of tested groups. Predominantly, adhesive failure was observed for all groups. CONCLUSIONS: Dentin surface treatment with sodium bicarbonate air abrasion improves bond strength of SbU, irrespective of adhesive application mode, which makes this approach an alternative to increase adhesive performance of Scotchbond Universal Adhesive to dentin.

Asunto(s)

Recubrimiento Dental Adhesivo/métodos , Recubrimientos Dentinarios/química , Dentina/efectos de los fármacos , Cementos de Resina/química , Temperatura , Preparación del Diente/métodos , Abrasión Dental por Aire/métodos , Análisis de Varianza , Resinas Compuestas/química , Fracaso de la Restauración Dental , Humanos , Ensayo de Materiales , Reproducibilidad de los Resultados , Bicarbonato de Sodio/química , Estadísticas no Paramétricas , Propiedades de Superficie/efectos de los fármacos , Resistencia a la Tracción

RESUMEN

Abstract Objectives: To evaluate the effects of dentin pretreatment and temperature on the bond strength of a universal adhesive system to dentin. Material and Methods: Ninety-six extracted non-carious human third molars were randomly divided into 12 groups (n=8) according to Scotchbond Universal Adhesive (SbU) applied in self-etch (SE) and etch-and-rinse (ER) mode, adhesive temperature (20°C or 37°C) and sodium bicarbonate or aluminum oxide air abrasion. After composite build up, bonded sticks with cross-sectional area of 1 mm2 were obtained to evaluate the microtensile bond strength (μTBS). The specimens were tested at a crosshead speed of 0.5 mm/min on a testing machine until failure. Fractured specimens were analyzed under stereomicroscope to determine the failure patterns in adhesive, cohesive (dentin or resin) and mixed fractures. The microtensile bond strength data was analyzed using two-way ANOVA and Tukey's test (α=5%). Results: Interaction between treatment and temperature was statistically significant for SbU applied in self-etch technique. Both dentin treatments showed higher bond strength for ER mode, regardless of adhesive temperature. When compared to control group, sodium bicarbonate increased bond strength of SbU in SE technique. Adhesive temperature did not significantly affect the μTBS of tested groups. Predominantly, adhesive failure was observed for all groups. Conclusions: Dentin surface treatment with sodium bicarbonate air abrasion improves bond strength of SbU, irrespective of adhesive application mode, which makes this approach an alternative to increase adhesive performance of Scotchbond Universal Adhesive to dentin.

Asunto(s)

Humanos , Temperatura , Recubrimiento Dental Adhesivo/métodos , Recubrimientos Dentinarios/química , Cementos de Resina/química , Preparación del Diente/métodos , Dentina/efectos de los fármacos , Propiedades de Superficie/efectos de los fármacos , Resistencia a la Tracción , Ensayo de Materiales , Reproducibilidad de los Resultados , Análisis de Varianza , Bicarbonato de Sodio/química , Estadísticas no Paramétricas , Resinas Compuestas/química , Fracaso de la Restauración Dental , Abrasión Dental por Aire/métodos

RESUMEN

ABSTRACT Objective The study aimed to evaluate effects of air abrasion with alumina or glass beads on bond strengths of resin cements to CAD/CAM composite materials. Material and Methods CAD/CAM composite block materials [Cerasmart (CS) and Block HC (BHC)] were pretreated as follows: (a) no treatment (None), (b) application of a ceramic primer (CP), (c) alumina-blasting at 0.2 MPa (AB), (d) AB followed by CP (AB+CP), and (e) glass-beads blasting at 0.4 MPa (GBB) followed by CP (GBB+CP). The composite specimens were bonded to resin composite disks using resin cements [G-CEM Cerasmart (GCCS) and ResiCem (RC)]. The bond strengths after 24 h (TC 0) and after thermal cycling (TC 10,000 at 4–60°C) were measured by shear tests. Three-way ANOVA and the Tukey compromise post hoc tests were used to analyze statistically significant differences between groups (α=0.05). Results For both CAD/CAM composite materials, the None group exhibited a significant decrease in bond strength after TC 10,000 (p<0.05). AB showed significantly higher bond strength after TC 10,000 than the None group, while CP did not (p<0.05). GBB exhibited smaller surface defects than did AB; however, their surface roughnesses were not significantly different (p>0.05). The AB+CP group showed a significantly higher bond strength after TC 10,000 than did the AB group for RC (p<0.05), but not for GCCS. The GBB+CP group showed the highest bond strength for both thermal cyclings (p<0.05). Conclusions Air abrasion with glass beads was more effective in increasing bond durability between the resin cements and CAD/CAM composite materials than was using an alumina powder and a CP.

Asunto(s)

Abrasión Dental por Aire/métodos , Óxido de Aluminio/química , Resinas Compuestas/química , Diseño Asistido por Computadora , Vidrio/química , Cementos de Resina/química , Análisis de Varianza , Cementación/métodos , Cerámica/química , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Reproducibilidad de los Resultados , Resistencia al Corte , Propiedades de Superficie , Factores de Tiempo

RESUMEN

PURPOSE: The objective of this study was to evaluate the microtensile bond strength (µTBS) of two resin cements bonded to dentin pre-treated with experimental niobophosphate bioactive glass (NBG). METHODS: The experimental bioactive glass was prepared by mixing different amounts of NbO5; (NH4)2HP4; CaO; Na2CO3. The particle size distribution and composition of the bioactive glass powder were determined. Twenty flat dentin surfaces from sound extracted human molars were polished with 600-grit SiC paper and air-abraded using experimental bioactive glass niobium powder. The bonding procedures were accomplished by the application of two resin cements: self-etching Panavia F or self-adhesive RelyX U-100. The resin-bonded specimens were cut and the µTBS test was performed after 24h. The failure mode was determined with a stereomicroscope at 40× magnification. The results were statistically analyzed by two-way ANOVA and Tukey tests (α=0.05). RESULTS: The two-way ANOVA did not detect interactions between factors, but only a difference between the self-etching and self-adhesive cement (p=0.001). The self-etching resin cement Panavia F obtained a higher µTBS than the self-adhesive cement Relyx U-100. The predominant failure mode of the cements was adhesive/mixed between the resin cement and dentin. CONCLUSION: A new bioactive glass containing niobium did not interfere with the immediate bonding performance of self-etching and self-adhesive cements.

Asunto(s)

Abrasión Dental por Aire/métodos , Recubrimiento Dental Adhesivo , Dentina , Vidrio , Cementos de Resina , Resinas Sintéticas , Resistencia a la Tracción , Vidrio/química , Humanos , Tamaño de la Partícula , Fosfatos

RESUMEN

OBJECTIVE: The study aimed to evaluate effects of air abrasion with alumina or glass beads on bond strengths of resin cements to CAD/CAM composite materials. MATERIAL AND METHODS: CAD/CAM composite block materials [Cerasmart (CS) and Block HC (BHC)] were pretreated as follows: (a) no treatment (None), (b) application of a ceramic primer (CP), (c) alumina-blasting at 0.2 MPa (AB), (d) AB followed by CP (AB+CP), and (e) glass-beads blasting at 0.4 MPa (GBB) followed by CP (GBB+CP). The composite specimens were bonded to resin composite disks using resin cements [G-CEM Cerasmart (GCCS) and ResiCem (RC)]. The bond strengths after 24 h (TC 0) and after thermal cycling (TC 10,000 at 4-60°C) were measured by shear tests. Three-way ANOVA and the Tukey compromise post hoc tests were used to analyze statistically significant differences between groups (α=0.05). RESULTS: For both CAD/CAM composite materials, the None group exhibited a significant decrease in bond strength after TC 10,000 (p<0.05). AB showed significantly higher bond strength after TC 10,000 than the None group, while CP did not (p<0.05). GBB exhibited smaller surface defects than did AB; however, their surface roughnesses were not significantly different (p>0.05). The AB+CP group showed a significantly higher bond strength after TC 10,000 than did the AB group for RC (p<0.05), but not for GCCS. The GBB+CP group showed the highest bond strength for both thermal cyclings (p<0.05). CONCLUSIONS: Air abrasion with glass beads was more effective in increasing bond durability between the resin cements and CAD/CAM composite materials than was using an alumina powder and a CP.

Asunto(s)

Abrasión Dental por Aire/métodos , Óxido de Aluminio/química , Resinas Compuestas/química , Diseño Asistido por Computadora , Vidrio/química , Cementos de Resina/química , Análisis de Varianza , Cementación/métodos , Cerámica/química , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Reproducibilidad de los Resultados , Resistencia al Corte , Propiedades de Superficie , Factores de Tiempo

RESUMEN

INTRODUCTION: The shear bond strength of orthodontic brackets bonded to micro-hybrid and micro-particulate resins under different surface treatment methods was assessed. METHODS: Two hundred and eighty test samples were divided into 28 groups (n = 10), where 140 specimens were filled with Durafill micro-particulate resin and 140 with Charisma composite. In 140 samples, a coupling agent (silane) was applied. The surface treatment methods were: Phosphoric and hydrofluoric acid etching, sodium bicarbonate and aluminum oxide blasting, stone and burs. A Universal Instron Machine was used to apply an occlusal shear force directly to the resin composite bracket surface at a speed of 0.5 mm/min. The means were compared using analysis of variance and multivariate regression to assess the interaction between composites and surface treatment methods. RESULTS: Means and standard deviations for the groups were: Sodium bicarbonate jet 11.27 ± 2.78; burs 9.26 ± 3.01; stone 7.95 ± 3.67; aluminum oxide blasting 7.04 ± 3.21; phosphoric acid 5.82 ± 1.90; hydrofluoric acid 4.54 ± 2.87, and without treatment 2.75 ± 1.49. An increase of 1.94 MPa in shear bond strength was seen in Charisma groups. Silane agent application reduced the Charisma shear bond strength by 0.68 Mpa, but increased Durafill means for bicarbonate blasting (0.83), burs (0.98) and stone drilling (0.46). CONCLUSIONS: The sodium bicarbonate blasting, burs and stone drilling methods produced adequate shear bond strength and may be suitable for clinical use. The Charisma micro hybrid resin composite showed higher shear bond means than Durafill micro particle composite.

Asunto(s)

Grabado Ácido Dental , Abrasión Dental por Aire/métodos , Recubrimiento Dental Adhesivo , Análisis del Estrés Dental , Soportes Ortodóncicos , Silanos , Análisis de Varianza , Resinas Compuestas , Análisis de Regresión , Resistencia al Corte , Bicarbonato de Sodio , Propiedades de Superficie

RESUMEN

This study evaluated 3 implant surfaces in a dog model: (1) resorbable-blasting media + acid-etched (RBMa), alumina-blasting + acid-etching (AB/AE), and AB/AE + RBMa (hybrid). All of the surfaces were minimally rough, and Ca and P were present for the RBMa and hybrid surfaces. Following 2 weeks in vivo, no significant differences were observed for torque, bone-to-implant contact, and bone-area fraction occupied measurements. Newly formed woven bone was observed in proximity with all surfaces.

Asunto(s)

Abrasión Dental por Aire/métodos , Implantes Dentales , Oseointegración , Implantes Absorbibles , Grabado Ácido Dental , Óxido de Aluminio , Animales , Implantación Dental Endoósea , Perros , Durapatita , Masculino , Propiedades de Superficie , Tibia/cirugía , Torque

RESUMEN

INTRODUCTION: The shear bond strength of orthodontic brackets bonded to micro-hybrid and micro-particulate resins under different surface treatment methods was assessed. METHODS: Two hundred and eighty test samples were divided into 28 groups (n = 10), where 140 specimens were filled with Durafill micro-particulate resin and 140 with Charisma composite. In 140 samples, a coupling agent (silane) was applied. The surface treatment methods were: Phosphoric and hydrofluoric acid etching, sodium bicarbonate and aluminum oxide blasting, stone and burs. A Universal Instron Machine was used to apply an occlusal shear force directly to the resin composite bracket surface at a speed of 0.5 mm/min. The means were compared using analysis of variance and multivariate regression to assess the interaction between composites and surface treatment methods. RESULTS: Means and standard deviations for the groups were: Sodium bicarbonate jet 11.27±2.78; burs 9.26±3.01; stone 7.95±3.67; aluminum oxide blasting 7.04±3.21; phosphoric acid 5.82±1.90; hydrofluoric acid 4.54±2.87, and without treatment 2.75±1.49. An increase of 1.94 MPa in shear bond strength was seen in Charisma groups. Silane agent application reduced the Charisma shear bond strength by 0.68 Mpa, but increased Durafill means for bicarbonate blasting (0.83), burs (0.98) and stone drilling (0.46). CONCLUSION: The sodium bicarbonate blasting, burs and stone drilling methods produced adequate shear bond strength and may be suitable for clinical use. The Charisma micro hybrid resin composite showed higher shear bond means than Durafill micro particle composite.

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INTRODUÇÃO: foram avaliadas as forças de cisalhamento após colagem de braquetes ortodônticos em superfícies resinosas microparticuladas ou micro-híbridas, após diferentes tratamentos de superfície. MÉTODOS: foram utilizados 280 corpos de prova, divididos em grupos de 10 elementos cada, sendo 140 preenchidos com resina microparticulada Durafill e 140 com resina micro-híbrida Charisma. Os tratamentos de superfície envolveram: ácido fosfórico, ácido fluorídrico, jato de bicarbonato de sódio, jato de óxido de alumínio, pedra e broca. A silanagem foi utilizada em metade dos grupos. O cisalhamento foi realizado com a máquina universal de testes EMIC DL 10000 MF, com célula de 10kg e velocidade de 0,5mm/min. As comparações entre as forças de cisalhamento foram obtidas por meio da análise de variância, e o grau de interação entre os tipos de compósito e o preparo de superfície foram obtidos por meio de uma regressão multivariada. RESULTADOS: as médias e desvios-padrão foram: jato de bicarbonato = 11,27 ± 2,78; broca = 9,26 ± 3,01; pedra = 7,95 ± 3,67; jato de óxido de alumínio = 7,04 ± 3,21; ácido fosfórico = 5,82 ± 1,90; ácido fluorídrico = 4,54 ± 2,87; e sem preparo = 2,75 ± 1,49. Um acréscimo de 1,94MPa foi obtido com o uso do compósito Charisma. A silanagem reduziu em 0,68MPa as médias do compósito Charisma, e aumentou o Durafill com uso do jato de bicarbonato (0,83), broca (0,98) e pedra (0,46). CONCLUSÃO: os preparos com jato de bicarbonato, broca e pedra obtiveram médias de forças apropriadas para colagem. O compósito Charisma apresentou forças de maior intensidade que as da resina Durafill.

Asunto(s)

Grabado Ácido Dental , Abrasión Dental por Aire/métodos , Recubrimiento Dental Adhesivo , Análisis del Estrés Dental , Soportes Ortodóncicos , Silanos , Análisis de Varianza , Resinas Compuestas , Análisis de Regresión , Resistencia al Corte , Bicarbonato de Sodio , Propiedades de Superficie

RESUMEN

UNLABELLED: Titanium reacts strongly with elements, mainly oxygen at high temperature. The high temperature of titanium laser welding modifies the surface, and may interfere on the metal-ceramic tensile bond strength. OBJECTIVE: The influence of laser welding on the titanium-ceramic bonding has not yet been established. The purpose of this in vitro study was to analyze the influence of laser welding applied to commercially pure titanium (CpTi) substructure on the bond strength of commercial ceramic. The influence of airborne particle abrasion (Al2O3) conditions was also studied. MATERIAL AND METHODS: Forty CpTi cylindrical rods (3 mm x 60 mm) were cast and divided into 2 groups: with laser welding (L) and without laser welding (WL). Each group was divided in 4 subgroups, according to the size of the particles used in airborne particle abrasion: A - Al2O3 (250 µm); B - Al2O3 (180 µm); C - Al2O3 (110 µm); D - Al2O3 (50 µm). Ceramic rings were fused around the CpTi rods. Specimens were invested and their tensile strength was measured at fracture with a universal testing machine at a crosshead speed of 2.0 mm/min and 200 kgf load cell. Statistical analysis was carried out with analysis of variance and compared using the independent t test (p<0.05). RESULTS: Significant differences were found among all subgroups (p<0.05). The highest and the lowest bond strength means were recorded in subgroups WLC (52.62 MPa) and LD (24.02 MPa), respectively. CONCLUSION: Airborne particle abrasion yielded significantly lower bond strength as the Al2O3 particle size decreased. Mechanical retention decreased in the laser-welded specimens, i.e. the metal-ceramic tensile bond strength was lower.

Asunto(s)

Abrasión Dental por Aire/métodos , Cerámica/química , Recubrimiento Dental Adhesivo/métodos , Soldadura Dental/métodos , Rayos Láser , Titanio/química , Análisis de Varianza , Ensayo de Materiales , Aleaciones de Cerámica y Metal/química , Microscopía Electrónica de Rastreo , Tamaño de la Partícula , Propiedades de Superficie , Resistencia a la Tracción

RESUMEN

Titanium reacts strongly with elements, mainly oxygen at high temperature. The high temperature of titanium laser welding modifies the surface, and may interfere on the metal-ceramic tensile bond strength. OBJECTIVE: The influence of laser welding on the titanium-ceramic bonding has not yet been established. The purpose of this in vitro study was to analyze the influence of laser welding applied to commercially pure titanium (CpTi) substructure on the bond strength of commercial ceramic. The influence of airborne particle abrasion (Al2O3) conditions was also studied. MATERIAL AND METHODS: Forty CpTi cylindrical rods (3 mm x 60 mm) were cast and divided into 2 groups: with laser welding (L) and without laser welding (WL). Each group was divided in 4 subgroups, according to the size of the particles used in airborne particle abrasion: A - Al2O3 (250 µm); B - Al2O3 (180 µm); C - Al2O3 (110 µm); D - Al2O3 (50 µm). Ceramic rings were fused around the CpTi rods. Specimens were invested and their tensile strength was measured at fracture with a universal testing machine at a crosshead speed of 2.0 mm/min and 200 kgf load cell. Statistical analysis was carried out with analysis of variance and compared using the independent t test (p<0.05). RESULTS: Significant differences were found among all subgroups (p<0.05). The highest and the lowest bond strength means were recorded in subgroups WLC (52.62 MPa) and LD (24.02 MPa), respectively. CONCLUSION: Airborne particle abrasion yielded significantly lower bond strength as the Al2O3 particle size decreased. Mechanical retention decreased in the laser-welded specimens, i.e. the metal-ceramic tensile bond strength was lower.

Asunto(s)

Abrasión Dental por Aire/métodos , Cerámica/química , Recubrimiento Dental Adhesivo/métodos , Soldadura Dental/métodos , Rayos Láser , Titanio/química , Análisis de Varianza , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Aleaciones de Cerámica y Metal/química , Tamaño de la Partícula , Propiedades de Superficie , Resistencia a la Tracción

RESUMEN

AIM: This study evaluated, by scanning electron microscope (SEM) and EDS, the effect of different strategies for silica coating (sandblasters, time and distance) of a glass-infiltrated ceramic (In-Ceram Alumina). METHODS: Forty-one ceramic blocks were produced. For comparison of the three air-abrasion devices, 15 ceramic samples were divided in three groups (N.=5): Bioart, Microetcher and Ronvig (air-abrasion parameters: 20 s at a distance of 10 mm). For evaluation of the time and distance factors, ceramic samples (N.=5) were allocated in groups considering three applied times (5 s, 13 s and 20 s) and two distances (10 mm and 20 mm), using the Ronvig device. In a control sample, no surface treatment was performed. After that, the micro-morphologic analyzes of the ceramic surfaces were made using SEM. EDS analyzes were carried out to detect the % of silica on representative ceramic surface. ANOVA and Tukey tests were used to analyze the results. RESULTS: One-way ANOVA showed the silica deposition was different for different devices (P=0.0054). The Ronvig device promoted the highest silica coating compared to the other devices (Tukey test). Two-way ANOVA showed the distance and time factors did not affect significantly the silica deposition (application time and distance showed no statistical difference). CONCLUSION: The Ronvig device provided the most effective silica deposition on glass-infiltrated alumina ceramic surface and the studied time and distance for air-abrasion did not affect the silica coating.

Asunto(s)

Abrasión Dental por Aire/instrumentación , Abrasión Dental por Aire/métodos , Cerámica , Dióxido de Silicio , Factores de Tiempo

RESUMEN

AIM: To evaluate the effect of prophylaxis using sodium bicarbonate and colored beverages on the color parameters of a resin composite. METHODS: Eighty specimens (Z350-3M ESPE) were randomly allocated into eight groups (n = 10), according to the combination of staining solution (artificial saliva, cola, red wine, or coffee) and air-powder abrasion with sodium bicarbonate (either performed or not performed). Specimens were immersed in the staining solution for 48 h (two 24-h cycles). Color evaluation was based on the CIELab system. Two measurements were carried out using a spectrophotometer (Commission Internationale de L'Eclairage L* a* b* system) before and after the immersion period. Final measurement data were analyzed by two-way anova/Tukey's test, and comparisons were made between initial and final measurements by anova/Dunnett's test, with a 5% significance level. RESULTS: Most comparisons between initial and final measurements were statistically significant. Red wine and coffee significantly affected the color parameters (L*, b*, and ΔE). However, only coffee significantly increased a* values. When compared with untreated surfaces, air-powder abrasion resulted in alterations of b* and a* parameters, but did not affect L* and ΔE. CONCLUSIONS: Both colored beverage solutions and air-powder abrasion can affect the color of composite resin restorations.

Asunto(s)

Abrasión Dental por Aire/métodos , Bebidas , Resinas Compuestas/química , Materiales Dentales/química , Bebidas Gaseosas , Café/química , Color , Colorimetría/métodos , Profilaxis Dental/métodos , Humanos , Inmersión , Ensayo de Materiales , Saliva Artificial/química , Bicarbonato de Sodio/química , Espectrofotometría/instrumentación , Propiedades de Superficie , Temperatura , Factores de Tiempo , Vino

RESUMEN

Dentinal surfaces prepared with air abrasion have considerably different characteristics from those prepared with conventional instruments. Different hybrid layer morphology and thickness occur, which can result in differences in the quality of restorations placed on dentinal surfaces prepared with a diamond bur compared to surfaces prepared using air abrasion. The objective of this study was to compare the hybrid layer thickness and morphology formed utilizing Scotchbond Multi-Purpose Plus (SBMP) on dentin prepared with a diamond bur in a high-speed handpiece and on dentin prepared using air abrasion. Flat dentin surfaces obtained from five human teeth were prepared using each method, then treated with the dentin adhesive system according to manufacturer's instructions. After a layer of composite was applied, specimens were sectioned, flattened, polished, and prepared for scanning electron microscopy. Ten different measurements of hybrid layer thickness were obtained along the bonded surface in each specimen. SBMP produced a 3.43 ± 0.75 µm hybrid layer in dentin prepared with diamond bur. This hybrid layer was regular and found consistently. In the air abrasion group, SBMP produced a 4.94 ± 1.28 µm hybrid layer, which was regular and found consistently. Statistical ANOVA (P = 0.05) indicated that there was a statistically significant difference between the groups. These data indicate that the air abrasion, within the parameters used in this study, provides a thick hybrid layer formation.

Asunto(s)

Abrasión Dental por Aire/métodos , Recubrimiento Dental Adhesivo/métodos , Preparación de la Cavidad Dental/métodos , Recubrimientos Dentinarios/química , Dentina/ultraestructura , Cementos de Resina/química , Resinas Compuestas/química , Preparación de la Cavidad Dental/instrumentación , Equipo Dental de Alta Velocidad , Materiales Dentales/química , Pulido Dental/métodos , Diamante/química , Humanos , Ensayo de Materiales , Microscopía Electrónica de Rastreo , Propiedades de Superficie

RESUMEN

This study evaluated the influence of surface treatment on the shear bond strength of a composite resin (CR), previously submitted to the application of a temporary cement (TC), to an adhesive luting cement. Eight-four CR cylinders (5 mm diameter and 3 mm high) were fabricated and embedded in acrylic resin. The sets were divided into 6 groups (G1 to G6) (n=12). Groups 2 to 6 received a coat of TC. After 24 h, TC was removed and the CR surfaces received the following treatments: G2: ethanol; G3: rotary brush and pumice; G4: air-abrasion; G5: air-abrasion and adhesive system; G6: air-abrasion, acid etching and adhesive system. G1 (control) did not receive TC or any surface treatment. The sets were adapted to a matrix and received an increment of an adhesive luting cement. The specimens were subjected to the shear bond strength test. ANOVA and Tukey's tests showed that G3 (8.53 MPa) and G4 (8.63 MPa) differed significantly (p=0.001) from G1 (13.34 MPa). The highest mean shear bond strength values were found in G5 (14.78 MPa) and G6 (15.86 MPa). Air-abrasion of CR surface associated with an adhesive system provided an effective bond of the CR to the adhesive luting cement, regardless the pre-treatment with the phosphoric acid.

Asunto(s)

Abrasión Dental por Aire/métodos , Resinas Compuestas , Recubrimiento Dental Adhesivo/métodos , Cementos Dentales , Resistencia al Corte , Análisis de Varianza , Restauración Dental Provisional/métodos , Análisis del Estrés Dental , Curación por Luz de Adhesivos Dentales , Estadísticas no Paramétricas , Propiedades de Superficie

RESUMEN

OBJECTIVE: To assess microleakage in conservative class V cavities prepared with aluminum-oxide air abrasion or turbine and restored with self-etching or etch-and-rinse adhesive systems. MATERIALS AND METHODS: Forty premolars were randomly assigned to 4 groups (I and II: air abrasion; III and IV: turbine) and class V cavities were prepared on the buccal surfaces. Conditioning approaches were: groups I/III - 37% phosphoric acid; groups II/IV - self-priming etchant (Tyrian-SPE). Cavities were restored with One Step Plus/Filtek Z250. After finishing, specimens were thermocycled, immersed in 50% silver nitrate, and serially sectioned. Microleakage at the occlusal and cervical interfaces was measured in mm and calculated by a software. Data were subjected to ANOVA and Tukey's test (α=0.05). RESULTS: Marginal seal provided by air abrasion was similar to high-speed handpiece, except for group I. There was SIGNIFICANT difference between enamel and dentin/cementum margins for to group I and II: air abrasion. The etch-and-rinse adhesive system promoted a better marginal seal. At enamel and dentin/cementum margins, the highest microleakage values were found in cavities treated with the self-etching adhesive system. At dentin/cementum margins, high-speed handpiece preparations associated with etch-and-rinse system provided the least dye penetration. CONCLUSION: Marginal seal of cavities prepared with aluminum-oxide air abrasion was different from that of conventionally prepared cavities, and the etch-and-rinse system promoted higher marginal seal at both enamel and dentin margins.

Asunto(s)

Abrasión Dental por Aire/métodos , Preparación de la Cavidad Dental/métodos , Filtración Dental/clasificación , Grabado Ácido Dental/métodos , Óxido de Aluminio/química , Resinas Compuestas/química , Recubrimiento Dental Adhesivo , Preparación de la Cavidad Dental/instrumentación , Cemento Dental/ultraestructura , Esmalte Dental/ultraestructura , Equipo Dental de Alta Velocidad , Adaptación Marginal Dental , Pulido Dental , Restauración Dental Permanente/métodos , Dentina/ultraestructura , Recubrimientos Dentinarios/química , Humanos , Ensayo de Materiales , Metacrilatos/química , Ácidos Fosfóricos/química , Tinción con Nitrato de Plata , Propiedades de Superficie , Temperatura

RESUMEN

OBJECTIVE: To assess microleakage in conservative class V cavities prepared with aluminum-oxide air abrasion or turbine and restored with self-etching or etch-and-rinse adhesive systems. Materials and Methods: Forty premolars were randomly assigned to 4 groups (I and II: air abrasion; III and IV: turbine) and class V cavities were prepared on the buccal surfaces. Conditioning approaches were: groups I/III - 37 percent phosphoric acid; groups II/IV - self-priming etchant (Tyrian-SPE). Cavities were restored with One Step Plus/Filtek Z250. After finishing, specimens were thermocycled, immersed in 50 percent silver nitrate, and serially sectioned. Microleakage at the occlusal and cervical interfaces was measured in mm and calculated by a software. Data were subjected to ANOVA and Tukey's test (α=0.05). RESULTS: Marginal seal provided by air abrasion was similar to high-speed handpiece, except for group I. There was SIGNIFICANT difference between enamel and dentin/cementum margins for to group I and II: air abrasion. The etch-and-rinse adhesive system promoted a better marginal seal. At enamel and dentin/cementum margins, the highest microleakage values were found in cavities treated with the self-etching adhesive system. At dentin/cementum margins, high-speed handpiece preparations associated with etch-and-rinse system provided the least dye penetration. CONCLUSION: Marginal seal of cavities prepared with aluminum-oxide air abrasion was different from that of conventionally prepared cavities, and the etch-and-rinse system promoted higher marginal seal at both enamel and dentin margins.

Asunto(s)

Humanos , Abrasión Dental por Aire/métodos , Preparación de la Cavidad Dental/métodos , Filtración Dental/clasificación , Grabado Ácido Dental/métodos , Óxido de Aluminio/química , Resinas Compuestas/química , Recubrimiento Dental Adhesivo , Equipo Dental de Alta Velocidad , Adaptación Marginal Dental , Pulido Dental , Preparación de la Cavidad Dental/instrumentación , Cemento Dental/ultraestructura , Esmalte Dental/ultraestructura , Restauración Dental Permanente/métodos , Recubrimientos Dentinarios/química , Dentina/ultraestructura , Ensayo de Materiales , Metacrilatos/química , Ácidos Fosfóricos/química , Tinción con Nitrato de Plata , Propiedades de Superficie , Temperatura

RESUMEN

Investigation of the effectiveness of surface treatments that promote a strong bond strength of resin cements to metals can contribute significantly to the longevity of metal-ceramic restorations. This study evaluated the effect of surface treatments on the shear bond strength (SBS) of a resin cement to commercially pure titanium (CP Ti). Ninety cast CP Ti discs were divided into 3 groups (n=30), which received one of the following airborne-particle abrasion conditions: (1) 50 microm Al(2)O(3) particles; (2) 30 microm silica-modified Al(2)O(3) particles (Cojet Sand); (3) 110 microm silica-modified Al(2)O(3) particles (Rocatec). For each airborne-particle abrasion condition, the following post-airborne-particle abrasion treatments were used (n=10): (1) none; (2) adhesive Adper Single Bond 2; (3) silane RelyX Ceramic Primer. RelyX ARC resin cement was bonded to CP Ti surfaces. All specimens were thermally cycled before being tested in shear mode. Failure mode was determined. The best association was Rocatec plus silane. All groups showed 100% adhesive failure. There were combinations that promote higher SBS than the protocol recommended by the manufacturer of RelyX ARC.

Asunto(s)

Abrasión Dental por Aire/métodos , Recubrimiento Dental Adhesivo , Fracaso de la Restauración Dental , Cementos de Resina/química , Titanio/química , Análisis de Varianza , Desconsolidación Dental , Restauración Dental Permanente/métodos , Análisis del Estrés Dental , Humanos , Tamaño de la Partícula , Resistencia al Corte , Estadísticas no Paramétricas , Estrés Mecánico , Propiedades de Superficie