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1.
Materials (Basel) ; 16(6)2023 Mar 16.
Artículo en Inglés | MEDLINE | ID: mdl-36984270

RESUMEN

This research studies the influence of the copper alloying of medium-carbon steel on mechanical properties after quenching and tempering at 500 °C. The microstructure was characterised using SEM, EBSD, TEM, and XRD analysis. The mechanical properties were comprehensively investigated using hardness measurements, tensile and Charpy impact tests and solid solution, grain boundary, dislocation, and precipitation strengthening contributions were estimated. Higher yield strength for Cu-alloyed steel was confirmed at about 35-73 MPa. The precipitation strengthening contribution from Cu precipitates in the range of 11-49 MPa was calculated. The interaction between Cu precipitates and dislocations retards the decrease in dislocation density. Similar values of effective grain size of martensite crystals were measured for Cu-alloyed and Cu-free steel as well. Copper alloyed steel exhibited significantly deteriorated impact toughness, total plastic elongation, and reduction of area. The size of Cu precipitates ranged from 8.3 nm after tempering at 500 °C for 6 h to 13.9 nm after tempering for 48 h.

2.
Materials (Basel) ; 13(11)2020 May 26.
Artículo en Inglés | MEDLINE | ID: mdl-32466388

RESUMEN

The temperature-dependent microstructural evolution and corresponding mechanical stability of retained austenite in medium-C TRIP-assisted 0.43C-1.45Mn-0.98Si-1Al-0.033Nb-0.01Ti steel obtained by thermomechanical processing was investigated using static tensile tests and microstructural studies. The light microscopy, image analysis, XRD diffraction and the Jaoul-Crussard analysis were applied to reveal relationships between microstructure and mechanical properties. Specimens were deformed in the static tensile tests in a temperature range of -20-140 °C. It was found that an increase in deformation temperature resulted in the reduced intensity of the TRIP effect due to the higher stability of retained austenite. An increase in the retained austenite stability along with a smaller grain size and a change from its blocky morphology to thin layers was also indicated. The impact of strengthening mechanisms at different temperatures was analyzed. The best combination of strength and ductility was obtained in the samples deformed at 20 and 60 °C, which is associated with the moderate work hardening in this temperature range. The Jaoul-Crussard analysis showed much less strengthening during the second phase of deformation at 100 and 140 °C due to the high stability of retained austenite. The higher C content in the investigated TRIP steel resulted in substantial volume fractions of retained austenite stable after completing deformation.

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