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1.
Sci Rep ; 14(1): 20797, 2024 Sep 05.
Artículo en Inglés | MEDLINE | ID: mdl-39242758

RESUMEN

The non-conventional manufacturing technologies are notorious when it comes to productivity and processing time in production-related industries. However, the aerospace and other high-end sectors enjoy another quality matrix of these processes and compromise on the processing time. For instance, the machinability of hard-to-cut materials such as Ti6Al4V aerospace alloy for micro-impressions is challenging and commonly carried out through non-conventional processes. Among these processes, the electric discharge machining (EDM) is famous for machining Ti6Al4V. In the current study, the EDM process is enhanced through modified dielectrics such as kerosene with non-ionic liquids (span 20, 60, and 80) and cryogenically treated tool electrodes (aluminum and graphite), and is compared to the conventional kerosene-based process. A three-phase experimental campaign is deployed to explore parametric effects including modified dielectric conditions (non-ionic liquid type and concentration), tool material, and machine parameter pulse ON:OFF time. A total of 60 experiments (54 modified dielectrics and 6 as baseline) were performed to explore process physics. The statistical analyses show that the unmodified process (kerosene dielectric-based) results in the least favorable results 0.58 mm3/min against cryo-graphite and 1.2 mm3/min against cryo-aluminum electrodes. However, the modified dielectrics outperform and improve process dynamics by altering dielectric conditions through hydrophilic-lipophilic balance. Surface morphological analysis shows significantly shallow craters on the machined surface showing evidence of effective flushing through a modified dielectric (S-20) as compared to a kerosene-based dielectric. A thorough microscopical, statistical, and scanning electron-based analysis is carried out to explain the process and correlate significant improvements.

2.
Ultrasonics ; 145: 107431, 2024 Sep 02.
Artículo en Inglés | MEDLINE | ID: mdl-39250841

RESUMEN

Sapphire ultrasonic vibration-assisted flexible polishing (UVAFP) is a promising technique for comprehensively improving the surface integrity of machined parts. The technique was performed on an ultra-precision machine tool with the in-situ monitoring systems in this paper, which aims to provide a new perspective for understanding the material removal mechanisms in the sapphire UVAFP process. A Taguchi L9 (43) orthogonal experiment was conducted to investigate the effects of feed distance, spindle speed, ultrasonic vibration (UV), and polishing time on the surface finish and material removal in the process. In addition, the effect of a polyurethane ball tool is not trivial. A single-factor experiment was conducted for exploring it. Based on a laser displacement measurement system and an acoustic emission sensor system, the characteristics of time-dependent ultrasonic amplitude and ultrasonic frequency for the sapphire UVAFP system were analyzed, with the effectiveness of UV demonstrated. Based on a three-component force measurement system, the characteristics of normal force and its relationship with process parameters and tool deformation were analyzed, with macro- and micro-level examined. In conclusion, this paper presents the characterization of UV and polishing force in the sapphire UVAFP process, providing novel insights into understanding the material removal mechanisms of sapphire and even more manufacturing problems.

3.
Data Brief ; 56: 110793, 2024 Oct.
Artículo en Inglés | MEDLINE | ID: mdl-39252783

RESUMEN

The turning process remains one of the most widely used manufacturing methods in the industry due to its high flexibility and production rates. Despite being an extensively used technique, the impact of this machining process on the surface integrity of the components has not yet been resolved in the literature, although it is well known that it can have a major influence on their final life. With the aim of providing new insights in the field, an extensive experimental campaign was designed on a 42CrMo4 quenched and tempered steel (in the following 42CrMo4+QT) using the response surface method. As inputs of this experimental design, the principal machining parameters were selected: feed rate (mm/rev), cutting speed (m/min), depth of cut (mm) and insert radius (mm). Meanwhile the main outputs measured where the surface roughness (µm) and the longitudinal residual stresses (MPa). In parallel, the turning operation of each specimen was monitored and the forces (X, Y and Z), current consumption of the main lathe motor, sound pressure and tool holder accelerations were recorded.

4.
J Conserv Dent Endod ; 27(7): 719-723, 2024 Jul.
Artículo en Inglés | MEDLINE | ID: mdl-39262601

RESUMEN

Aim: The objective of the present research was to assess and compare the residual dentin thickness after biomechanical preparation of teeth using three distinct rotary nickel-titanium (Ni-Ti) file systems. Materials and Methods: In the current experimental study, a total of 45 single-rooted teeth were selected for the analysis. The cementoenamel junction of each tooth was decoronated using a diamond disc. The teeth were randomly allocated to three groups, with each group representing a different rotary file system: Group 1: Hero GOLD (Micro Mega), Group 2: One Curve (Micro Mega), and Group 3: HyFlex electro-discharge machining (EDM) (Coltene-Whaledent, Altstatten, Switzerland). To evaluate the initial condition of the teeth, cone-beam computed tomography (CBCT) scans were conducted before the biomechanical preparation. The teeth were positioned on a modeling wax sheet, and the CBCT scans provided baseline measurements. The biomechanical preparation of the root canals followed the manufacturer's recommended guidelines for each file system. After the completion of the canal preparation, follow-up CBCT scans were conducted. The postprocedure CBCT scans were then compared with the initial scans to assess any changes in the residual thickness of dentin in the teeth. Statistical Analysis: Post hoc Tukey analysis of variance tests was utilized to examine differences between the groups. A statistically significant result was defined as P = 0.05 or less for every test. Results: The comparison of preinstrumentation and postinstrumentation CBCT images showed that the HyFlex EDM group removed less dentin clinically compared to the other two groups, i.e., Hero GOLD and One Curve. No significant statistical difference was found between Hero GOLD versus One Curve, One Curve versus HyFlex EDM, and Hero GOLD versus HyFlex EDM. Conclusion: Based on the results of this study, the HyFlex EDM file system exhibited superior cutting efficiency at various levels. Nonetheless, additional investigations are required to comprehensively assess the influence of Ni-Ti rotary file systems on the remaining dentin thickness.

5.
Angew Chem Int Ed Engl ; : e202412876, 2024 Aug 02.
Artículo en Inglés | MEDLINE | ID: mdl-39092533

RESUMEN

The high-rate electrochemical dissolution of copper in nitrate electrolytes is investigated primarily via polarization curves, while varying parameters such as the electrolyte flow velocity, the electrolyte resistance, the anode geometry, and the temperature. This study focuses on the re-rise in current at high voltages after the limiting current plateau. As a result of the studies, a change in the complexation mechanism from hydration to "solvo-nitration" is proposed, which requires an additional potential drop within the electrochemical double layer.

6.
Sci Rep ; 14(1): 19228, 2024 08 20.
Artículo en Inglés | MEDLINE | ID: mdl-39164355

RESUMEN

For successful treatment of diseases, sufficient therapeutics must be provided to the body. Microneedle applications in therapeutic delivery and analytics sampling are restricted because of various issues, including smaller area for drug loading and analytics sampling. To achieve sufficient drug loading and analytics sampling and improve drug penetration while maintaining painless administration, patch-type microneedle arrays were designed and fabricated using polymer casting from a conical cavity mold. Microcavities were formed on a carbon plate via micromechanical machining. A porous polymer layer was coated on a microneedle patch (MNP). The pores of the porous polymer layer provided space and channels for drug delivery. A pH-sensitive polymer layer was employed to cap the porous polymer layer, which prevented drug leakage during storage and provided a stimulus drug release in response to body pH conditions. The drug can be delivered through holes connected to both sides of the patch. The drug release of the MNP was investigated in vitro and in vivo and showed conceptual proof that these MNs have the potential to enhance treatment protocols for various diseases with the flexibility of coating and therapeutic materials and offer significant scope for further variations and advancement.


Asunto(s)
Carbono , Sistemas de Liberación de Medicamentos , Agujas , Sistemas de Liberación de Medicamentos/métodos , Carbono/química , Animales , Liberación de Fármacos , Microinyecciones/instrumentación , Microinyecciones/métodos , Porosidad , Concentración de Iones de Hidrógeno , Polímeros/química , Ratones
7.
Sensors (Basel) ; 24(15)2024 Jul 23.
Artículo en Inglés | MEDLINE | ID: mdl-39123824

RESUMEN

In this work, we investigate the impact of annotation quality and domain expertise on the performance of Convolutional Neural Networks (CNNs) for semantic segmentation of wear on titanium nitride (TiN) and titanium carbonitride (TiCN) coated end mills. Using an innovative measurement system and customized CNN architecture, we found that domain expertise significantly affects model performance. Annotator 1 achieved maximum mIoU scores of 0.8153 for abnormal wear and 0.7120 for normal wear on TiN datasets, whereas Annotator 3 with the lowest expertise achieved significantly lower scores. Sensitivity to annotation inconsistencies and model hyperparameters were examined, revealing that models for TiCN datasets showed a higher coefficient of variation (CV) of 16.32% compared to 8.6% for TiN due to the subtle wear characteristics, highlighting the need for optimized annotation policies and high-quality images to improve wear segmentation.

8.
Adv Healthc Mater ; : e2402531, 2024 Aug 05.
Artículo en Inglés | MEDLINE | ID: mdl-39104021

RESUMEN

A reliable method for fabricating biomimetic scaffolds with a controllable mineral gradient to facilitate the surgical repair of tendon-to-bone injuries and the regeneration of the enthesis is reported. The gradient in mineral content is created by sequentially spin-coating with hydroxyapatite/poly(ε-caprolactone) suspensions containing hydroxyapatite nanoparticles in decreasing concentrations. To produce pores and facilitate cell infiltration, the spin-coated film is released and patterned with an array of funnel-shaped microchannels by laser machining. The unique design provided both mechanical (i.e., substrate stiffness) and biochemical (e.g., hydroxyapatite content) cues to spatially control the graded differentiation of mesenchymal stem cells. Immunocytochemical analysis of human mesenchymal stem cell-seeded scaffolds after 14 days of culture demonstrated the formation of a spatial phenotypic cell gradient from osteoblasts to mineralized chondrocytes based on the level of mineralization in the scaffold. By successfully recreating compositional and cellular features of the native tendon enthesis, the biomimetic scaffolds offer a promising avenue for improved tendon-to-bone repair.

9.
Polymers (Basel) ; 16(15)2024 Jul 30.
Artículo en Inglés | MEDLINE | ID: mdl-39125192

RESUMEN

In this paper, a new method involving a wear-resistant and reusable template is proposed for the preparation of high-mechanical-strength superhydrophobic polymer film based on wire electrical discharge machining (WEDM). A solid-liquid-contact-angle simulation model was established to obtain surface-texture types and sizes that may achieve superhydrophobicity. The experimental results from template preparation show that there is good agreement between the simulation and experimental results for the contact angle. The maximum contact angle on the template can reach 155.3° given the appropriate triangular surface texture and WEDM rough machining. Besides, the prepared superhydrophobic template exhibits good wear resistance and reusability. PDMS superhydrophobic polymer films were prepared by the template method, and their properties were tested. The experimental results from the preparation of superhydrophobic polymer films show that the maximum contact angle of the polymer films can be up to 154.8° and that these films have good self-cleaning and anti-icing properties, wear resistance, bending resistance, and ductility.

10.
Micromachines (Basel) ; 15(8)2024 Jul 24.
Artículo en Inglés | MEDLINE | ID: mdl-39203598

RESUMEN

These days, metal matrix composites (MMCs) are being widely utilized in automotive and aerospace industries as prominent alternatives to traditional materials. Owing to their elevated strength-to-weight proportion, exceptional fracture toughness, and lightweight design, they can be used in a variety of applications. MMCs undergo extensive machining while making parts and components out of them. The machining of monolithic materials, such as metals and alloys, is a widely used and established process in different industries, such as the aerospace, bio-medical, and automotive sectors. Because of the properties of the metal matrix and the strong reinforcement, MMCs provide unique challenges. Modern machining processes have been found to be superior in overcoming challenges and achieving improved machinability of MMCs. An overview of MMC machining with modern methods is provided in this article. This article first outlines MMCs and addresses the need for and difficulties associated with their machining. Next, it reviews previous investigations on the machining of MMCs employing modern methods like electrical discharge machining, laser machining, abrasive machining, and hybrid machining. Productivity and surface integrity issues, including delamination and roughness, etc., are discussed. When presenting the review, the benefits and drawbacks of modern processes are also taken into account.

11.
Micromachines (Basel) ; 15(8)2024 Jul 30.
Artículo en Inglés | MEDLINE | ID: mdl-39203633

RESUMEN

The piezoelectric effect refers to a physical phenomenon where piezoelectric materials generate an electric field when subjected to mechanical stress or undergo mechanical deformation when subjected to an external electric field. This principle underlies the operation of piezoelectric sensors. Piezoelectric sensors have garnered significant attention due to their excellent self-powering capability, rapid response speed, and high sensitivity. With the rapid development of sensor techniques achieving high precision, increased mechanical flexibility, and miniaturization, a range of flexible electronic products have emerged. As the core constituents of piezoelectric sensors, flexible piezoelectric composite materials are commonly used due to their unique advantages, including high conformability, sensitivity, and compatibility. They have found applications in diverse domains such as underwater detection, electronic skin sensing, wearable sensors, targeted therapy, and ultrasound diagnostics for deep tissue. The advent of flexible piezoelectric composite materials has revolutionized the design concepts and application scenarios of traditional piezoelectric materials, playing a crucial role in the development of next-generation flexible electronic products. This paper reviews the research progress on flexible piezoelectric composite materials, covering their types and typical fabrication techniques, as well as their applications across various fields. Finally, a summary and outlook on the existing issues and future development of these composite materials are provided.

12.
Micromachines (Basel) ; 15(8)2024 Aug 01.
Artículo en Inglés | MEDLINE | ID: mdl-39203653

RESUMEN

In order to introduce the magnetic field into micro electrical machining technology to explore the influence of magnetic field on micro electrical machining, the development of a precision controllable magnetic field-assisted platform is particularly important. This platform needs to precisely control the spatial magnetic field. This study first completes the hardware design and construction of the magnetic field generation device, using electromagnetic coils with soft iron cores as the sources of the magnetic field. Mathematical models of the magnetic field are established and calibrated. Since the magnetic dipole model cannot effectively describe the magnetic field generated by the electromagnetic coil, this study adopts a more precise description method: the spherical harmonic function expansion model and the magnetic multipole superposition model. The calibration of the magnetic field model is based on actual excitation magnetic field data, so a magnetic field sampling device is designed to obtain the excitation magnetic field of the workspace. The model is calibrated based on a combination of the theoretical model and magnetic field data, and the performance of the constructed setup is analyzed. Finally, a magnetic field-assisted platform has been developed which can generate magnetic fields in any direction within the workspace with intensities ranging from 0 to 0.2 T. Its magnetic field model arrives at an error percentage of 2.986%, a variance of 0.9977, and a root mean square error (RMSE) of 0.71 mT, achieving precise control of the magnetic field in the workspace.

13.
Micromachines (Basel) ; 15(8)2024 Aug 09.
Artículo en Inglés | MEDLINE | ID: mdl-39203672

RESUMEN

BK7 glass, with its outstanding mechanical strength and optical performance, plays a crucial role in many cutting-edge technological fields and has become an indispensable and important material. These fields have extremely high requirements for the surface quality of BK7 glass, and any small defects or losses may affect its optical performance and stability. However, as a hard and brittle material, the processing of BK7 glass is extremely challenging, requiring precise control of machining parameters to avoid material fracture or excessive defects. Therefore, how to obtain the required surface quality with lower cost machining techniques has always been the focus of researchers. This article introduces the properties, application background, machining methods, material removal mechanism, and surface and subsurface damage of optical glass BK7 material. Finally, scientific predictions and prospects are made for future development trends and directions for improvement of BK7 glass machining.

14.
Micromachines (Basel) ; 15(8)2024 Aug 14.
Artículo en Inglés | MEDLINE | ID: mdl-39203681

RESUMEN

The production of many components used in MEMS or NEMS devices, especially those with com-plex shapes, requires machining as the best option among manufacturing techniques. Ultraprecision machining is normally employed to achieve the required shapes, dimensional accuracy, or improved surface quality in most of these devices and other areas of application. Compared to conventional machining, ultraprecision machining involves complex phenomenal processes that require extensive investigations for a better understanding of the material removal mechanism. Materials such as semiconductors, composites, steels, ceramics, and polymers are commonly used, particularly in devices designed for harsh environments or applications where alloyed metals may not be suitable. However, unlike alloyed metals, materials like semiconductors (e.g., silicon), ceramics (e.g., silicon carbide), and polymers, which are typically brittle and/or hard, present significant challenges. These challenges include achieving precise surface integrity without post-processing, managing the ductile-brittle transition, and addressing low material removal rates, among others. This review paper examines current research trends in mechanical ultraprecision machining and sustainable ultraprecision machining, along with the adoption of molecular dynamics simulation at the micro and nano scales. The identified challenges are discussed, and potential solutions for addressing these challenges are proposed.

15.
Polymers (Basel) ; 16(16)2024 Aug 21.
Artículo en Inglés | MEDLINE | ID: mdl-39204581

RESUMEN

CO2 laser machining is a cost effective and time saving solution for fabricating microchannels on polymethylmethacrylate (PMMA). Due to the lack of research on the incubation effect and ablation behavior of PMMA under high-power laser irradiation, predictions of the microchannel profile are limited. In this study, the ablation process and mechanism of a continuous CO2 laser machining process on microchannel production in PMMA in single-pass and multi-pass laser scan modes are investigated. It is found that a higher laser energy density of a single pass causes a lower ablation threshold. The ablated surface can be divided into three regions: the ablation zone, the incubation zone, and the virgin zone. The PMMA ablation process is mainly attributed to the thermal decomposition reactions and the splashing of molten polymer. The depth, width, aspect ratio, volume ablation rate, and mass ablation rate of the channel increase as the laser scanning speed decreases and the number of laser scans increases. The differences in ablation results obtained under the same total laser energy density using different scan modes are attributed to the incubation effect, which is caused by the thermal deposition of laser energy in the polymer. Finally, an optimized simulation model that is used to solve the problem of a channel width greater than spot diameter is proposed. The error percentage between the experimental and simulation results varies from 0.44% to 5.9%.

16.
ACS Biomater Sci Eng ; 10(8): 5381-5389, 2024 Aug 12.
Artículo en Inglés | MEDLINE | ID: mdl-39041183

RESUMEN

In this research, we investigate the impact of varying machining parameters [depth of cutting (mm) and spindle rotation speed (rpm)] on the microstructure and electrochemical behavior of Ti6Al4V-ELI dental implants. This comprehensive study employs an approach, leveraging potentiodynamic methods and electrochemical impedance spectroscopy, to analyze corrosion behavior in a phosphate-buffered saline solution. To further deepen our understanding of corrosion kinetics, we used an alternating current circuit model, based on a simple Randles equivalent circuit. This model elucidates the corrosion interface interactions of the Ti6Al4-V-ELI alloy implant within the PBS solution. In addition, our research delves into the microstructural implications of different machining parameters, utilizing scanning electron microscopy and X-ray diffraction (XRD) techniques to reveal significant phase changes. The changes in texture were examined qualitatively by comparing the intensities of the peaks of the XRD pattern. A detailed correlation analysis further links the machining parameters with the corrosion properties of dental implants, offering a comprehensive perspective rarely explored in the existing literature. The results obtained for the three samples showed that the corrosion resistance would be higher by increasing the machining depth and the spindle rotation and that the corrosion current would be lower. As a result, a lower corrosion rate was obtained. Finally, experimental results from electrochemical analyses are compared and discussed.


Asunto(s)
Aleaciones , Implantes Dentales , Titanio , Corrosión , Titanio/química , Aleaciones/química , Ensayo de Materiales , Difracción de Rayos X , Microscopía Electrónica de Rastreo , Espectroscopía Dieléctrica , Diseño de Prótesis Dental , Propiedades de Superficie
17.
Materials (Basel) ; 17(14)2024 Jul 19.
Artículo en Inglés | MEDLINE | ID: mdl-39063874

RESUMEN

The paper investigates various methods of microfinishing and arrives at the best technique to produce a very smooth surface. Various setups, with and without oscillation, were developed, together with a microfinishing attachment used on conventional lathes and milling machines. The workpiece material used was an amorphous nickel-phosphorus Ni-P alloy. The surface roughness parameters, such as Sa, Sv, and Sp, were measured with the TalySurf CCI6000 instrument. For the measurement of the surface protrusions, an "analysis of islands" technique was used at various levels of cut-off. The 2BA method-machining below the workpiece axis with oscillation-turned out to be the most effective method applied because it had the highest density of protrusions while having the smallest value of surface roughness. Non-oscillation with the machining zone below the axis also becomes effective, indicating that repositioning can compensate for a lack of oscillation. Already, the very compact surface structure achieved with minimized depths in the valleys by the 2BA method supported the improvement in tribological performance and increase in load-carrying capacity, together with lubricant retention enhancement. These results show that the microfinishing process can be optimized by parameter tuning, and also, non-oscillating methods could come to be a practical alternative, probably reducing the complexity of equipment and cutting costs. Further studies need to be aimed at the scalability of these methods and their application to other materials and fields.

18.
Micromachines (Basel) ; 15(7)2024 Jul 20.
Artículo en Inglés | MEDLINE | ID: mdl-39064437

RESUMEN

To solve the problems of poor surface quality and low tool life in conventional machining (CM) of AerMet100 steel, an experimental study was conducted in laser-assisted machining (LAM) of AerMet100 steel. The effects of laser power, cutting speed, feed rate, and depth of cut on the surface roughness of AerMet100 steel were studied based on a single-factor experiment. The degree of influence of each factor on the surface roughness was evaluated by analyses of variance and range in the orthogonal experiment, and the combination of process parameters for the optimal surface roughness was obtained. The order of influence was as follows: laser power > cutting speed > depth of cut > feed rate; the optimal combination of process parameters was laser power 200 W, cutting speed 56.5 m/min, feed rate 0.018 mm/rev, and depth of cut 0.3 mm. Compared to CM, the surface morphology of the workpiece under the optimization of LAM was relatively smooth and flat, the surface roughness Ra was 0.402 µm, which was reduced by 62.11%, the flank wear was reduced from 208.69 µm to 52.17 µm, there were no tipping or notches, and the tool life was significantly improved. The study shows that the LAM of AerMet100 steel has obvious advantages in improving surface quality and reducing tool wear.

19.
Environ Sci Pollut Res Int ; 31(35): 47584-47597, 2024 Jul.
Artículo en Inglés | MEDLINE | ID: mdl-39002084

RESUMEN

In the manufacturing processes, consideration of sustainability is of particular importance. The current study is concerned with the influences of changing the process variables on the reduction of pollutions in the wood-CNC machining operation. Noise and dust are the studied pollutants in the present research work. Process variables include feed rate, spindle speed, step-over, and depth of cut, and the aim is to predict the behavior of aforementioned pollutants variations in the current process. The amounts of these harmful factors are measured based on existing standards. In order to analyze the findings, adaptive neuro-fuzzy inference system (ANFIS) and regression analysis methods have been employed, separately. The effects of process parameters on response variables have been comprehensively studied. The research findings demonstrated that for the present problem, ANFIS outcomes are more accurate. According to the mean absolute error (MAE) criterion, the prediction errors of ANFIS for noise and dust factors were computed to, in turn, 0.50 and 14.89. Meanwhile, the error values for prediction of noise and dust responses using regression analysis were calculated as 1.54 and 34.62, respectively.


Asunto(s)
Polvo , Ruido , Madera , Polvo/análisis , Análisis de Regresión , Monitoreo del Ambiente
20.
Heliyon ; 10(11): e31772, 2024 Jun 15.
Artículo en Inglés | MEDLINE | ID: mdl-38841480

RESUMEN

Electrical discharge machining with solid electrodes represents an efficient solution to generate blind cavities with complex geometry. Vegetable oils represent an alternative to conventional dielectrics, which are considered harmful for the environment and human health. This study tested the feasibility of two widely used vegetable oils, sunflower and soybean, under intense machining of three alloys with application in aeronautic industry, aiming for high process productivity and a good surface quality. The results have revealed that vegetable oils are capable to ensure an improvement of the material removal rates that can reach up to 55.15 % compared to mineral oil. Also, the vegetable dielectrics allowed an improvement of surface quality for non-ferrous alloys, up to a maximum of 19.70 %, whereas for the stainless steel, the mineral oil has provided a better surface finish.

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