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Assembling atomic layers of van der Waals materials (vdW) combines the physics of two materials, offering opportunities for novel functional devices. Realization of this has been possible because of advancements in nanofabrication processes which often involve chemical processing of the materials under study; this can be detrimental to device performance. To address this issue, we have developed a modified micro-manipulator setup for cryogenic exfoliation, pick up, and transfer of vdW materials to assemble heterostructures. We use the glass transition of a polymer PDMS to cleave a flake into two, followed by its pick-up and drop to form pristine twisted junctions. To demonstrate the potential of the technique, we fabricated twisted heterostructure of Bi2Sr2CaCu2O8+x (BSCCO), a van der Waals high-temperature cuprate superconductor. We also employed this method to re-exfoliate NbSe2 and make twisted heterostructure. Transport measurements of the fabricated devices indicate the high quality of the artificial twisted interface. In addition, we extend this cryogenic exfoliation method for other vdW materials, offering an effective way of assembling heterostructures and twisted junctions with pristine interfaces.
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REBCO has been used extensively as coated conductors applied to superconducting magnets due to its exceptional superconducting properties. As a REBCO superconductor, YbBa2Cu3O7-y (Yb123) has a low melting temperature, making it suitable for use as an intermediate medium connector while preparing the superconducting joint. However, there is still uncertainty about the formation mechanism of Yb123 and the synthesis of this superconductor has not been fully understood. Therefore, this study systematically investigated the phase transformation process of Yb123 during heat treatment in flowing oxygen. The results indicated that Yb123 sample with the highest phase purity could be obtained by annealing at 927 °C or 937 °C but not in between, respectively. Furthermore, a quantitative phase analysis revealed that the sample annealed at 937 °C had a phase purity greater than 80 wt%. Additionally, a strong c-axis texture was observed in the bulk Yb123 superconductor prepared at 937 °C. Meanwhile, the superconducting results revealed that the bulk sample's Tc was 89.9 K, and its self-field critical current densities at 4.2 K and 77 K were 1.3 × 105 A/cm2 and 5.0 × 103 A/cm2, respectively. Based on the results mentioned above, the phase transformation process and formation mechanism of Yb123 in flowing oxygen were elaborated.
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High-temperature superconductor (HTS) bulks have demonstrated extremely intriguing potential for industrial and commercial applications due to their capability to trap significantly larger magnetic fields than conventional permanent magnets. The magnetic field in electrical rotating machines is a combination of alternating and rotational fields. In contrast, all previous research on the characterization of electromagnetic properties of HTS have solely engrossed on the alternating AC magnetic fields and the associated AC loss. This research paper gives a thorough examination of the AC loss measurement under various conditions. The obtained results are compared to the finite element-based H-formulation. The AC loss is measured at various amplitudes of circular flux density patterns and compared with the AC loss under one-dimensional alternating flux density. The loss variation has also been studied at other frequencies. The findings in this research paper provide more insights into material characterization, which will be useful in the design of future large-scale HTS applications.
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High-temperature cuprate superconductors based van der Waals (vdW) heterostructures hold high technological promise. One of the obstacles hindering their progress is the detrimental effect of disorder on the properties of the vdW-devices-based Josephson junctions (JJs). Here, a new method of fabricating twisted vdW heterostructures made of Bi2 Sr2 CuCa2 O8+δ , crucially improving the JJ characteristics and pushing them up to those of the intrinsic JJs in bulk samples, is reported. The method combines cryogenic stacking using a solvent-free stencil mask technique and covering the interface by insulating hexagonal boron nitride crystals. Despite the high-vacuum condition down to 10-6 mbar in the evaporation chamber, the interface appears to be protected from water molecules during the in situ metal deposition only when fully encapsulated. Comparing the current-voltage curves of encapsulated and unencapsulated interfaces, it is revealed that the encapsulated interfaces' characteristics are crucially improved, so that the corresponding JJs demonstrate high critical currents and sharpness of the superconducting transition comparable to those of the intrinsic JJs. Finally, it is shown that the encapsulated heterostructures are more stable over time.
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The iron-based superconductors are an ideal platform to reveal the enigma of the unconventional superconductivity and potential topological superconductivity. Among them, the monolayer Fe(Se,Te)/SrTiO3(001), which is proposed to be topological nontrivial, shows interface-enhanced high-temperature superconductivity in the two-dimensional limit. However, the experimental studies on the superconducting pairing mechanism of monolayer Fe(Se,Te) films are still limited. Here, by measuring the quasiparticle interference in monolayer Fe(Se,Te)/SrTiO3(001), we report the observation of the anisotropic structure of the large superconducting gap and the sign change of the superconducting gap on different electron pockets. The results are well consistent with the "bonding-antibonding" s±-wave pairing symmetry driven by spin fluctuations in conjunction with spin-orbit coupling. Our work is of basic significance not only for a unified superconducting formalism in the iron-based superconductors, but also for understanding of topological superconductivity in high-temperature superconductors.
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We argue that the current carrying properties of high-temperature superconducting thin films can be further improved, in particular under the mid-field range (B ≈ 0.1-2 T), via introduction of multilayer structures that compromise between good zero field critical current and vortex pinning performance. In this work we focus on a simple bilayer structure consisting of two adjacent layers of pure YBa2Cu3O6+x(YBCO) and BaZrO3(BZO) doped YBCO under magnetic field within the mid-field range oriented parallel to thec-axis of the YBCO unit cell. We have utilized a computational model to simulate the vortex dynamics limited critical current separately from the associated zero field current, which is addressed analytically. The obtained results have allowed us to estimate the optimal layer thicknesses as a function of magnetic field. Our idealized model suggests that the thickness of the doped layer should be substantially smaller than the undoped one, that is around 30% of the total thickness of the film. We have estimated that the current carrying capability of the optimized bilayer structure can be up to 50% higher when compared with corresponding single layer films. Possible deviations from the obtained results associated with the idealized model, most prominently the effect of natural defects, are comprehensively discussed. Our results provide the foundation for the future experimental realization of the proposed bilayer structures. The comparison between the presented results and experimental realization would enable further study of the underlying primitive vortex interactions.
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Why are the transition temperatures (T c) of superconducting materials so different? The answer to this question is not only of great significance in revealing the mechanism of high-T c superconductivity but also can be used as a guide for the design of new superconductors. However, so far, it is still challenging to identify the governing factors affecting the T c. In this work, with the aid of machine learning and first-principles calculations, we found a close relevance between the upper limit of the T c and the energy-level distribution of valence electrons. It implies that some additional inter-orbital electron-electron interaction should be considered in the interpretation of high-T c superconductivity.
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This article reports on the non-trivial suppression of superconductivity in the Eu1-xPrxBCO cuprates. As non-magnetic Eu3+ ions are replaced by Pr3+ carrying a magnetic moment, spin-related superconductivity loss can be expected. The research shows that the superconductivity disappearance for x > 0.4 results from depletion of the carriers and their localization. The above conclusion was drawn by low-temperature X-ray diffraction analysis showing increased characteristic phonon frequencies with Pr content. This mechanism should promote electron-phonon coupling, at least for acoustic phonons. However, the inverse phenomenon was detected. Namely, there is a gradual deterioration of the optical phonons responsible for vibration of the Cu-O bonds with Pr increasing, as evidenced by Raman spectroscopy. Furthermore, the results of X-ray absorption spectroscopy precisely showed the location of the carriers for Pr-rich specimens. Finally, a schematic diagram for Eu1-xPrxBCO is proposed to consolidate the presented research.
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Nuclear magnetic resonance (NMR) probes using thin-film high temperature superconducting (HTS) resonators offer high sensitivity and are particularly suitable for small-sample applications. We are developing an improved 1.5 mm HTS NMR probe designed for operation at 14.1 T and optimized for 13C detection. The total sample volume is about 35 µL and the active sample volume is 20 µL. The probe employs HTS resonators for 13C and 1H transmission and detection and the 2H lock. We examine the interactions of multiple superconducting resonators and normal metal tuning loops on coil resonance frequency and probe sensitivity. We test a recently introduced 13C resonator design, engineered to significantly increase 13C detection sensitivity over previous all-HTS probes. At zero field, we observe a 13C quality factor of 6000 which is several times higher than previous resonators. In this work the coil design considerations and probe build-out procedure are discussed.
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The radiation intensity from the intrinsic Josephson junction high-Tc superconductor Bi2Sr2CaCu2O8+δ terahertz emitters (Bi2212-THz emitters) is one of the most important characteristics for application uses of the device. In principle, it would be expected to be improved with increasing the number of intrinsic Josephson junctions N in the emitters. In order to further improve the device characteristics, we have developed a stand alone type of mesa structures (SAMs) of Bi2212 crystals. Here, we understood the radiation characteristics of our SAMs more deeply, after we studied the radiation characteristics from three SAMs (S1, S2, and S3) with different thicknesses. Comparing radiation characteristics of the SAMs in which the number of intrinsic Josephson junctions are N⼠1300 (S1), 2300 (S2), and 3100 (S3), respectively, the radiation intensity, frequency as well as the characteristics of the device working bath temperature are well understood. The strongest radiation of the order of few tens of microwatt was observed from the thickest SAM of S3. We discussed this feature through the N2-relationship and the radiation efficiency of a patch antenna. The thinner SAM of S1 can generate higher radiation frequencies than the thicker one of S3 due to the difference of the applied voltage per junctions limited by the heat-removal performance of the device structures. The observed features in this study are worthwhile designing Bi2212-THz emitters with better emission characteristics for many applications.
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The three-band Emery model is applied to study the selected principal features of thed-wavesuperconducting phase in the copper-based compounds. The electron-electron correlations are taken into account by the use of the diagrammatic expansion of the Guztwiller wave function (DE-GWF method). The nodal Fermi velocity, Fermi momentum, and effective mass are all determined in the paired state and show relatively good agreement with the available experimental data, as well as with the corresponding single-band calculations. Additionally, the influence of the next-nearest neighbor oxygen-oxygen hopping and intersite Coulomb repulsion terms on the superconducting phase is analyzed.
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High-temperature superconductors (HTSs) are important for potential applications and for understanding the origin of strong correlations. Bi2 Sr2 CaCu2 O8+δ (BSCCO), a van der Waals material, offers a platform to probe the physics down to a unit-cell. Guiding the flow of electrons by patterning 2DEGS and oxide heterostructures has brought new functionality and access to new science. Similarly, modifying superconductivity in HTS locally, on a small length scale, is of immense interest for superconducting electronics. A route to modify superconductivity locally by depositing metal on the surface is reported here by transport studies on few unit-cell thick BSCCO. Deposition of chromium (Cr) on the surface over a selected area of BSCCO results in insulating behavior of the underlying region. Cr locally depletes oxygen in CuO2 planes and disrupts the superconductivity in the layers below. This technique of modifying superconductivity is suitable for making sub-micrometer superconducting wires and more complex superconducting devices.
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We calculate the effects of doping nanostructuration and the patterning of thin films of high-temperature superconductors (HTS) with the aim of optimizing their functionality as sensing materials for resistive transition-edge bolometer devices (TES). We focus, in particular, on spatial variations of the carrier doping into the CuO 2 layers due to oxygen off-stoichiometry, (that induce, in turn, critical temperature variations) and explore following two major cases of such structurations: First, the random nanoscale disorder intrinsically associated to doping levels that do not maximize the superconducting critical temperature; our studies suggest that this first simple structuration already improves some of the bolometric operational parameters with respect to the conventional, nonstructured HTS materials used until now. Secondly, we consider the imposition of regular arrangements of zones with different nominal doping levels (patterning); we find that such regular patterns may improve the bolometer performance even further. We find one design that improves, with respect to nonstructured HTS materials, both the saturation power and the operating temperature width by more than one order of magnitude. It also almost doubles the response of the sensor to radiation.
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Replacing normal metal NMR coils with thin-film high-temperature superconductor (HTS) resonators can significantly improve the sensitivity of analytical NMR. To study the use of these resonators for excitation as well as detection, we investigated the radio frequency properties of the HTS NMR coils in both frequency and time domain at a variety of transmit power levels. Experiments were conducted on a double-sided, counter wound spiral resonator designed to detect NMR signals from 13C nuclei at 14.1 T. Power-dependent nonlinearity was observed in the transmission coefficient and quality factor. The ability of the HTS resonators to accurately generate short pulses was studied in the time domain over the range power levels. The results of this study show that some form of Q switching is needed to get good transmit performance from HTS coils for 13C. For that purpose, the effect of adding a shorted transmission line stub to improve the pulse shapes and reduce phase transients was studied.
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Three topics concerning future hardware development for clinical MRI are discussed, with the general theme of operational simplification.
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Superconductors are essential in many present and future technologies, from large-scale devices for medical imaging, accelerators, or fusion experiments to ultra-low-power superconducting electronics. However, their potential applicability, and particularly that of high-temperature superconductors (HTS), is severely affected by limited performances at large magnetic fields and high temperatures, where their use is most needed. One of the main reasons for these limitations is the presence of quantized vortices, whose movements result in losses, internal noise, and reduced performances. The conventional strategy to overcome the flow of vortices is to pin them along artificial defects. Here, we theoretically and experimentally demonstrate that critical-current density in high-temperature superconductors can reach unprecedented high values at high fields and temperatures by preventing vortex entry. By tailoring the geometry, that is, reducing the width, W, of nanowire-patterned HTS films, the range of the Meissner state, for which no vortices are present, is extended up to very large applied field values, on the order of â¼1 T. Current densities on the order of the depairing current can be sustained under high fields for a wide range of temperatures. Results may be relevant both for devising new conductors carrying depairing-current values at high temperatures and large magnetic fields and for reducing flux noise in sensors and quantum systems.
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We present assembly and test results of a 3-nested-coil 800-MHz (18.8 T) REBCO insert (H800) for the MIT 1.3 GHz LTS/HTS NMR magnet currently under completion. Each of the three H800 coils is a stack of no-insulation (NI) REBCO double-pancake coils (DPs). The innermost 8.7-T Coil 1 (26 DPs) was completed by mid-2016; the middle 5.6-T Coil 2 (32 DPs) was complet-ed in mid-2017; while the outermost 4.5-T Coil 3 (38 DPs) was completed in early 2018. Coils 1, 2 & 3 were assembled together in early 2018 as a 3-nested-coil, the H800, and tested, first in liquid nitrogen to a power supply current of 20 A, followed by testing in liquid helium to a power supply current of 251.3 A, the H800's design operating current. After roughly five minutes settling time at 251.3 A, the H800 quenched. In this paper we examine probable sources of quench initiation and simulate ensuing quench behavior. Remedial efforts to minimize the tendency towards quenching in the H800 are presented and discussed.
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We present post-quench analyses of the MIT 800-MHz REBCO insert magnet (H800), unexpectedly quenched during operation in March 2018, and design study of a new 800-MHz HTS insert (H800N). The as-wound H800 was supposed to contribute 18.7 T and, with an LTS background magnet (L500), produce 30.5 T corresponding to a proton resonance frequency of 1.3 GHz. The H800 was operated at 4.2 K in liquid helium and, about 5 minutes after the power supply reached a target operating current of 251.3 A, it experienced a quench. Because the damage in the H800 was more widespread than it first appeared, we decided to design and build a new insert magnet, H800N. In designing H800N, we try to eliminate unanticipated flaws in our H800 design. H800N is to be more stable not to quench and more reliably survive against quench without permanent damage by: 1) adopting a single solenoid structure composed of 40 stacked double pancake coils with improved cross-over sections; 2) enhancing thermal stability; and 3) reducing excessive current margin for quench protection.
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Compact tokamak fusion reactors using advanced high-temperature superconducting magnets for the toroidal field coils have received considerable recent attention due to the promise of more compact devices and more economical fusion energy development. Facilities with combined fusion nuclear science and Pilot Plant missions to provide both the nuclear environment needed to develop fusion materials and components while also potentially achieving sufficient fusion performance to generate modest net electrical power are considered. The performance of the tokamak fusion system is assessed using a range of core physics and toroidal field magnet performance constraints to better understand which parameters most strongly influence the achievable fusion performance. This article is part of a discussion meeting issue 'Fusion energy using tokamaks: can development be accelerated?'.
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Research in the 1970s and 1980s by Sykes, Peng, Jassby and others showed the theoretical advantage of the spherical tokamak (ST) shape. Experiments on START and MAST at Culham throughout the 1990s and 2000s, alongside other international STs like NSTX at the Princeton Plasma Physics Laboratory, confirmed their increased efficiency (namely operation at higher beta) and tested the plasma physics in new regimes. However, while interesting devices for study, the perceived technological difficulties due to the compact shape initially prevented STs being seriously considered as viable power plants. Then, in the 2010s, high-temperature superconductor (HTS) materials became available as a reliable engineering material, fabricated into long tapes suitable for winding into magnets. Realizing the advantages of this material and its possibilities for fusion, Tokamak Energy proposed a new ST path to fusion power and began working on demonstrating the viability of HTS for fusion magnets. The company is now operating a compact tokamak with copper magnets, R0 â¼ 0.4 m, R/ a â¼ 1.8, and target Ip = 2MA, Bt0 = 3 T, while in parallel developing a 5 T HTS demonstrator tokamak magnet. Here we discuss why HTS can be a game-changer for tokamak fusion. We outline Tokamak Energy's solution for a faster way to fusion and discuss plans and progress, including benefits of smaller devices on the development path and advantages of modularity in power plants. We will indicate some of the key research areas in compact tokamaks and introduce the physics considerations behind the ST approach, to be further developed in the subsequent paper by Alan Costley. This article is part of a discussion meeting issue 'Fusion energy using tokamaks: can development be accelerated?'.