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1.
Microsc Res Tech ; 87(6): 1210-1221, 2024 Jun.
Artículo en Inglés | MEDLINE | ID: mdl-38308481

RESUMEN

Aluminium (Al) and magnesium (Mg) alloys are extensively used in the automobile sector because of their high strength-to-weight ratio, excellent castability low density and simplicity of recycling. Al-Mg structures used in the automotive sector can potentially reduce their weight. Although there is a significant opportunity for substantial cost reduction, the use of magnesium in aluminium structures remains restricted. This study aims to weld 3 mm-thick rolled sheets of AA6061 Al and AZ31B Mg alloy using the cold metal transfer (CMT) arc welding process. Three different filler wires (ER1100, ER4043, and ER5356) were used in the experiment. In this article, the mechanical and microstructure characteristics of Al/Mg dissimilar joints manufactured by CMT are evaluated and discussed in detail. Optical microscope (OM), scanning electron microscopy (SEM), energy dispersive x-ray spectroscopy (EDX), and x-ray diffraction (XRD) were used to analyze the CMT-welded Al/Mg dissimilar joints. Of the three filler wires used, ER4043 (Al-5%Si) filler wire yielded defect-free sound joints due to the presence of Si, which improves the flow ability of molten filler during welding. The presence of Mg-rich intermetallics-Al12Mg17) and Al-rich intermetallics-Al3Mg2 were observed. The fractured area of the CMT-welded Al/Mg dissimilar joints revealed the presence of the Mg-rich intermetallics (Al12Mg17), which is responsible for the decrease in tensile strength. The reduction of intermetallics, particularly of Mg-rich intermetallics (Al12Mg17) is important for improving joint strength. RESEARCH HIGHLIGHTS: Cold metal transfer (CMT) arc welding was used to control the Al-Mg-rich intermetallics in the Al/Mg dissimilar joints. The microstructure, morphology and phase composition of the welded joints were studied by OM, SEM, TEM, EDS and XRD. The weld metal and AL substrate bonded with a strong interface, while weld metal and Mg substrate were joined at the epitaxial solidification area where the intermetallic compounds of Mg2Al3, Mg17Al12 and Mg2Si are generated. The weld metal on the Mg side experienced brittle fracture, with a continuous distribution of Mg2Al3, Mg17Al12 and Mg2Si.

2.
Materials (Basel) ; 16(17)2023 Aug 30.
Artículo en Inglés | MEDLINE | ID: mdl-37687649

RESUMEN

The aim of this paper is to analyse the mechanical properties of butt joints between S355 steel and 6061-T6 aluminium alloy, as well as their relationship to changes in the structure of the material caused by welding. The effect of the tool offset was analysed in particular. For the analysis, tensile tests were carried out using macro- and mini-specimens taken from S355/AA6061-T6 joints and base materials. In addition, the macro- and microstructure of the joints was determined, the hardness profiles in the joints were analysed, and fractographic analysis of the fractures of the specimens was carried out. Based on the results of the macro- and microstructure examinations, typical friction stir welding (FSW) joint zones were characterised. The microstructure was observed in the interface line of the materials on the root side, the negative effect of which on the quality of the joint was confirmed by digital image correlation (DIC) strain analysis during the monotonic tensile test. The highest average value of su = 141 MPa for the entire joint was obtained for a 0.4 mm tool offset. The highest average value of su = 185 MPa for the selected joint layer was obtained for a 0.3 mm tool offset. Fracturing of the joint in the selected layer for the tool offset values of 0.3 mm and 0.4 mm occurred in the weld nugget zone (WNZ) where the lowest hardness was recorded.

3.
Materials (Basel) ; 16(8)2023 Apr 12.
Artículo en Inglés | MEDLINE | ID: mdl-37109869

RESUMEN

Ultrasonic metal welding (USMW) is widely used in assembling lithium-ion (Li-ion) battery packs due to its advantages in joining dissimilar and conductive materials in the solid state. However, the welding process and mechanisms are not yet clearly understood. In this study, dissimilar joints of aluminum alloy EN AW 1050 to copper alloy EN CW 008A were welded by USMW to simulate the tab-to-bus bar interconnects for Li-ion battery assembly. Qualitative and quantitative investigations were carried out on plastic deformation, microstructural evolution, and the correlated mechanical properties. During USMW, the plastic deformation concentrated on the Al side. The thickness of Al was reduced by more than 30%; complex dynamic recrystallization and grain growth occurred near the weld interface. The mechanical performance of the Al/Cu joint was evaluated with the tensile shear test. The failure load gradually increased until a welding duration of 400 ms, and then remained almost constant. The obtained results showed that the mechanical properties were greatly influenced by plastic deformation and microstructure evolution, which provides guidance for improving the weld quality and the process in general.

4.
Materials (Basel) ; 16(7)2023 Mar 30.
Artículo en Inglés | MEDLINE | ID: mdl-37049067

RESUMEN

Dissimilarities in metal laser welding lead to brittleness in welded joints due to differences in the thermophysical and chemical properties between dissimilar base materials. To overcome such brittleness, the addition of a preset coating onto the base materials as an interlayer is a method for attaining reliable welded joints. Nd:YAG laser butt welding of DP590 dual-phase steel and 304 stainless, both with a thickness of 1 mm, was performed with a preset nickel coating as an interlayer using an electroplating process. The relationship between the microstructure and the mechanical properties of the welded joints was researched, the microstructure and composition of the weldment were analyzed, and the microhardness, tensile strength and corrosion resistance were tested. The results showed that the preset nickel coating increased the content of Ni element in the welded joints, which is beneficial to the formation of lath martensite. The average hardness of the welded joints increased by 12%, and the tensile strength was higher than 370 MPa. The corrosion rate of the welded joints can be slowed down, and the corrosion resistance can be improved by increasing the nickel coating.

5.
Materials (Basel) ; 15(17)2022 Aug 26.
Artículo en Inglés | MEDLINE | ID: mdl-36079283

RESUMEN

In engineering applications, such as automobile, marine, aerospace, and railway, lightweight alloys of aluminum (Al) and magnesium (Mg) ensure design fitness for fuel economy, better efficiency, and overall cost reduction. Friction stir welding (FSW) for joining dissimilar materials has been considered better than the conventional fusion welding process because of metallurgical concerns. In this study, dissimilar joints were made between the AA6061 (A), AZ31B (B), and AZ91D (C) combinations based on the varying advancing side (AS) and retreating side (RS). The dissimilar joints prepared by the FSW process were further characterized by tensile testing, impact testing, corrosion testing, fracture, and statistical and cost analysis. The results revealed a maximum tensile strength of 192.39 MPa in AZ91 and AZ31B, maximum yield strength of 134.38 MPa in a combination of AA6061 and AZ91, maximum hardness of 114 Hv in AA6061 and AZ31B, and lowest corrosion rate of 7.03 mV/A in AA6061 and AZ31B. The results of the properties were supported by photomicrographic fracture analysis by scanning electron microscopy (SEM) observations. Further, the performance of dissimilar joints was statistically analyzed and prioritized for preference by similarity to the ideal solution (TOPSIS) method.

6.
Materials (Basel) ; 15(1)2021 Dec 21.
Artículo en Inglés | MEDLINE | ID: mdl-35009180

RESUMEN

In order to clarify the microstructural evolution and the mechanical property of dissimilar friction stir-welded joints of ZK60 and Mg-4.6Al-1.2Sn-0.7Zn magnesium alloys, two types of arrangement with ZK60 at advancing side (AS) or retreating side (RS) were adopted. The macrostructure and the microstructure of the dissimilar welded joints were discussed, and the microhardness and the transverse tensile properties of the joints were measured. There are three stirring sub-zones with different compositions and two clear interfaces within the joints. Due to the effect of both the original grain size of base materials and the growth of recrystallized grains, in the stir zone (SZ), the grain size of ZK60 increased slightly, while the grain size of Mg-4.6Al-1.2Sn-0.7Zn decreased significantly. The dissolution of precipitates was gradually significant from RS to AS within the SZ due to the gradual increase in strain and heat. The grain refinement led to an increase in hardness, while the dissolution of precipitates resulted in a decrease in hardness. The performance of the joints obtained with ZK60 placed on the RS is slightly better than that of that on the AS. The tensile fracture of both joints occurred at the interface between SZ and the thermos-mechanical affected zone at the AS, and showed a quasi-dissociative fracture.

7.
Materials (Basel) ; 13(12)2020 Jun 17.
Artículo en Inglés | MEDLINE | ID: mdl-32560372

RESUMEN

Laser penetration welding of magnesium alloys and pure titanium TA2 with unequal thickness was performed. Mg base metal with different Al content (AZ31B, AZ61A, AZ91D) was used to investigate the influence of Al element in microstructure and mechanical properties of Mg/Ti dissimilar joints. The results revealed that the change of Mg base metal did not influence the weld appearance of the joints. Three kinds of joint all presented the best mechanical property when the laser power was 3500 W. With the increase content of Al elements in Mg base metal, a reaction layer was observed which was identified as Ti3Al. The highest enrichment of Al element was obtained and its fraction reached 19.31 at% at the AZ91/TA2 interface. The chemical potential gradient of Al from AZ91 to Ti alloy was higher than that from the other two base metals based on thermodynamic calculation. The maximum fracture load reached 3597 N when AZ61 was employed as the base metal and the fracture position was the Ti base metal. AZ31/TA2 joints failed at the weld seam without necking due to the rapid propagation of cracks at the Mg/Ti interface. The AZ91/TA2 joint failed inside the Mg fusion zone with necking at the middle area of the weld, which resulted from the precipitation of brittle phases such as Mg-Al, Ti-Al phases in the fusion zone of Mg alloys.

8.
Materials (Basel) ; 13(3)2020 Feb 08.
Artículo en Inglés | MEDLINE | ID: mdl-32046295

RESUMEN

The present work describes the influence of the parameters employed in the gas tungsten arc welding process (GTAW) when nickel powder is used as a filler metal in 2304/2507 duplex stainless-steel dissimilar joints. Multi-objective optimization was applied in order to maintain the austenite/ferrite percentage in the welded zone. A microstructural and phase quantification analysis was performed in each sample through optical and scanning electron microscopes. It was found that a nickel powder addition combined with low heat input increased the biphasic ratio across the different zones of the dissimilar welded samples. Although the austenite volume fraction increased in the 2304 heat-affected zone (HAZ) near to 25%, it was not sufficient according to international standards. The obtained results led to the maintenance of the 50/50 phase percentage in the 2507 HAZ welded joint side, as well as to the increment of the austenite percentage in the 2304 HAZ.

9.
Materials (Basel) ; 12(7)2019 Apr 03.
Artículo en Inglés | MEDLINE | ID: mdl-30987253

RESUMEN

Friction stir welding (FSW) with a Zr interlayer was employed to join dissimilar alloys of 6061 Al and AZ31 Mg. The microstructures of Al/Mg and Al/Zr/Mg joints were investigated by optical microscopy (OM), scanning electron microscopy (SEM), and energy dispersive X-ray spectrometer (EDS). The results showed that the central part of the Zr interlayer was smashed and intermixed with the base materials in the stir zone, whereas the undamaged part remained stable at the Al/Mg interface. The formation of Al-Mg intermetallic compounds (IMCs) was suppressed by the Zr interlayer due to its synergetic effects of chemical modification and thermal barrier. The electrochemical measurements revealed a differentiated corrosion behavior for each joint, where the corrosion rate of representative regions increased in the order of Al alloy < Mg alloy < heat-affected zone < stir zone. The immersion tests indicated an enhancement in corrosion resistance for the Al/Zr/Mg joint compared with the Al/Mg joint, which is owing to the mitigated galvanic corrosion between the base materials by the Zr interlayer.

10.
Materials (Basel) ; 12(2)2019 Jan 09.
Artículo en Inglés | MEDLINE | ID: mdl-30634455

RESUMEN

In this paper, dissimilar Al⁻Cu joints of AA1050H/C1100-Cu, AA6061-T6/C1100-Cu, and AA1050H/C2600-brass are successfully welded by a friction stir welding (FSW) process. The aim of the present study is not only to examine the tensile strength, but also to investigate the reliability, durability, and failure behaviors of joints as correlated with the metallurgical bonded microstructures of varied Al⁻Cu joints. Experimental evidence confirms that good welding quality for an FSW Al⁻Cu dissimilar joint is obtained when pure Cu and brass plates are positioned at the advancing side. Cross-sectional microstructures reveal that the AA6061-T6/C1100-Cu joint exhibits an extensive metallurgical bonded region with significant onion rings in the welding zone, whereas the AA1050H/C2600-brass joint generally displays a clear mechanical kissing bonded boundary at the joint interface. Al2Cu, Al4Cu9, and γ-Cu5Zn8 are major intermetallic compounds (IMCs) that are formed within the metallurgical bonded welding zone. The Weibull model provides a statistical method for assessing the failure mechanism of FSW Al⁻Cu joints. Better welding reliability and tensile properties with ductile dimpled ruptures are obtained for the Al⁻Cu joints with a typical metallurgical bonded zone. However, a mechanical kissing bonded interface and thick interfacial IMCs result in the deterioration of tensile strength with a brittle fracture and a rapid increase in the failure probability of Al⁻Cu joints.

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