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Colloids Surf B Biointerfaces ; 111: 179-87, 2013 Nov 01.
Artículo en Inglés | MEDLINE | ID: mdl-23807127

RESUMEN

The degradation behavior of a MAO-AZ91D with a calcium phosphate/chitosan composite coating in the modified simulated human body fluid (m-SBF) was investigated by immersion experiments and electrochemical impedance spectroscopy. The compositions of the composite coating soaked in the m-SBF for different time intervals were studied by X-ray diffraction, Fourier transform infrared spectroscopy, Raman spectroscopy, thermo-gravimetric analysis and differential thermal analysis. The microstructures of the composite coating at different soaking stages were observed by using a scanning electron microscope. Results show that the as-prepared composite coating could slow down the corrosion rate of the AZ91D alloy and it demonstrated good bioactivity in the m-SBF. The coating's morphology changed from a flake-like one into a spherical-shaped one with the increase of immersion time in the m-SBF.


Asunto(s)
Aleaciones/química , Líquidos Corporales/química , Fosfatos de Calcio/química , Quitosano/química , Materiales Biocompatibles Revestidos/química , Espectroscopía Dieléctrica , Análisis Diferencial Térmico , Humanos , Concentración de Iones de Hidrógeno , Oxidación-Reducción , Espectroscopía Infrarroja por Transformada de Fourier , Termogravimetría , Difracción de Rayos X
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