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2.
Biomed Mater Eng ; 7(4): 265-70, 1997.
Artículo en Inglés | MEDLINE | ID: mdl-9408578

RESUMEN

Articulating paper/film is a sheet strip that is coated with ink- or dye-containing wax and is used for marking occlusal contacts and monitoring the results. New types of occlusal film systems have been developed recently, which are capable of being computer-interfaced to identify the occlusal contact points and digitize the occlusal force. The mechanical ductility and thickness of these occlusal sheets constitute some of their important properties. The objective of this study was to evaluate seven different occlusal sheets and compare their bulge ductility and thickness. A custom-designed photo-sensing bulge tester was used. Three paper-based sheets (BAP, BET and SFA), two plastic-based sheets (ACF and AOS), and advanced systems (TSS and FDP) were tested. The specimen size was 20 mm square. Fifteen samples were tested for each material. The sheet film thickness with coated layers was as follows: BAP, 62 microns; BET, 46 microns; SFA, 133 microns; ACF, 23 microns; AOS, 14 microns; TSS, 134 microns; and FDP, 82 microns. Ductility (standard deviation) was as follows: BAP, 2.10 (0.0060)%; BET, 2.14 (0.008)%; SFA, 5.19 (0.57)%; ACF, 8.68 (0.05)%; AOS, 16.26 (0.41)%; TSS, 16.26 (0.41)%; and FDP, 6.37 (0.09)%. One-way ANOVA analysis indicated that (1) there in no statistical difference between BAP and BET (p > 0.001), (2) there is a statistical difference (p < 0.001) among all the rest of the tested occlusal sheets, and (3) bulge ductility appears to be linearly related to film thickness, its correlation depending upon types of base materials.


Asunto(s)
Oclusión Dental Balanceada , Ajuste Oclusal/métodos , Papel/normas , Plásticos/normas , Colorantes , Humanos , Procesamiento de Imagen Asistido por Computador , Tinta , Ensayo de Materiales , Fotograbar , Ceras
3.
Biomed Mater Eng ; 7(5): 327-43, 1997.
Artículo en Inglés | MEDLINE | ID: mdl-9457383

RESUMEN

Acrylic resins are commonly used in many dental applications; especially in the fabrication of provisional fixed partial dentures. Among noticed technical drawbacks associated with this material are unsatisfactory mechanical properties. Moreover, if acrylic resins are exposed to moist environment, water sorption results in further mechanical deterioration. In order to improve the mechanical properties, aluminum, magnesium, and zirconium oxide powders and pulverized E-glass particles were separately admixed with pre-polymerized acrylic resin beads prior to mixing with monomer liquid. Particle loading ratios were 1, 2 and 3 vol.% with respect to pre-polymerized beads. Poly(methyl methacrylate), poly(ethyl methacrylate) and poly(isobutyl methacrylate) were used as resin matrices. Furthermore, a metal primer agent was employed in order to form a strong interphase between admixed particles and polymer matrix phase. Samples were subjected to three-point transverse bending tests at a crosshead speed of 10 mm/min. It was concluded that (1) addition of particles generally increases the water sorbed by the composite resins systems, (2) however, two vol.% admixtures in a PMMA resin matrix showed significant improvements in the mechanical properties (p < 0.05), (3) among the oxide particles, zirconia exhibited the greatest improvements in modulus of elasticity, transverse strength, toughness and hardness, and (4) mechanical properties (transverse strength, 0.2% offset yield strength and modulus of elasticity) were linearly correlated to hardness numbers.


Asunto(s)
Resinas Acrílicas/química , Dentadura Parcial Fija , Dentadura Parcial Provisoria , Óxido de Aluminio/química , Análisis de Varianza , Fenómenos Químicos , Química Física , Resinas Compuestas/química , Diseño de Dentadura , Elasticidad , Vidrio/química , Dureza , Óxido de Magnesio/química , Ensayo de Materiales , Metacrilatos/química , Metilmetacrilatos/química , Docilidad , Ácidos Polimetacrílicos/química , Polimetil Metacrilato/química , Estrés Mecánico , Agua/química , Circonio/química
4.
Biomed Mater Eng ; 7(5): 345-55, 1997.
Artículo en Inglés | MEDLINE | ID: mdl-9457384

RESUMEN

In Part I, it was found that (i) 2 vol.% admixture of reinforcing elements in PMMA (Jet) resin matrix had a significant beneficial effects on the mechanical properties, and (ii) among these, zirconia exhibited the greatest improvements in modulus of elasticity, transverse strength, toughness, and hardness number. Using the best combination (i.e., PMMA resin matrix and 2 vol.% ZrO2), exothermic temperature raise and polymerization shrinkage were further investigated. Deterioration in mechanical properties due to prolonged water sorption were also studied for 5 weeks. The following can be concluded: (1) By increasing liquid/powder ratio for PMMA control samples, the peak temperature occurrence was retarded by 3 min and raised by 8 degrees C. (2) The effect of admixed oxide particles to PMMA resin matrix or the heat generated during polymerization was not significant. (3) The polymerization volumetric shrinkage was influenced by the a mixture of particles, with increases as large as 0.9% (or 0.3% in linear shrinkage). (4) PMMA resin admixed with 2 vol.% of zirconia particles showed a continuous weight gain due to water sorption, mechanical properties appears to be increasing up to 1-week sorption, followed by rapid drop of all properties. (5) Autopolymerizing acrylic resins are a resin-resin composite material of pre-polymerized beads embedded in a newly formed acrylic matrix. The main fracture modality appears to occur through the matrix and at the interface, although some trans-beads fractures were identified. (6) It was suggested that incorporating certain type of oxide particles into the pre-polymerized beads would provide stronger resin matrix.


Asunto(s)
Resinas Acrílicas/química , Dentadura Parcial Fija , Dentadura Parcial Provisoria , Polimetil Metacrilato/química , Circonio/química , Óxido de Aluminio/química , Fenómenos Químicos , Química Física , Resinas Compuestas/química , Elasticidad , Vidrio/química , Dureza , Calor , Óxido de Magnesio/química , Ensayo de Materiales , Metacrilatos/química , Microscopía Electrónica de Rastreo , Docilidad , Polímeros/química , Polvos , Soluciones , Estrés Mecánico , Propiedades de Superficie , Temperatura , Factores de Tiempo , Agua/química
5.
Biomed Mater Eng ; 7(2): 111-9, 1997.
Artículo en Inglés | MEDLINE | ID: mdl-9262824

RESUMEN

Currently acrylic resins are commonly employed in many medical applications, especially for the fabrication of long span provisional restorations in dentistry and bone cement in orthopedics. On of the major problems associated with the conventional type of acrylic resins is their unsatisfactory mechanical properties. Among many attempts to strengthen acrylic resins, it has been demonstrated that they can be strengthened through the addition of reinforcement(s) as structural components of different size, shape and chemical composition, dispersed in the acrylic matrix, thus forming a composite structure. In the course of studies to strengthen dental polymeric resins by admixing various metallic oxide particles, PMMA-, PEMA-, and PIMA-based resins were reinforced by 2 vol.% added alumina, magnesia, zirconia, and silica powders. It was found that PMMA admixed with 2 vol.% zirconia exhibited the best improvement of mechanical properties (breaking strength, modulus of elasticity, offset yield strength, and fracture toughness as well). All tests were conducted under three-point bending. It was also found that the breaking strength based on the original sample dimension was, at most 20% less than those based on the final sample dimension. Moreover, this discrepancy was independent of the type of tested material, but dependent on the sample's modulus of elasticity.


Asunto(s)
Ensayo de Materiales , Polímeros , Resinas Sintéticas , Análisis de Varianza , Elasticidad , Tamaño de la Partícula , Estrés Mecánico
7.
J Prosthet Dent ; 76(2): 181-6, 1996 Aug.
Artículo en Inglés | MEDLINE | ID: mdl-8820811

RESUMEN

This article describes the use of a device for assisting in identification of the direction of the arc of rotation while locating the transverse horizontal opening and closing axis of the mandible. Translucent disks are mounted on the point of the styli of a kinematic face-bow and centering magnets are aligned with them, with no overlapping of the colors. The direction of the arcing movement is enlarged by the overlapping of the translucent disk over the centering magnet. The different color value generated by the overlapping identifies the arcing direction. After correction on the microadjustable arm, the centering magnet is realigned on the translucent disk. This sequence is repeated until the disk no longer overlaps with the centering magnet during the opening and closing movements of the mandible. This device uses the different color generated by mixing the color of the disk against a template of darker color. The disk enlarges the point of the stylus, thus magnifies the direction of the arc of rotation, and potentially reduces the clinical time necessary to locate the points of pure rotation.


Asunto(s)
Articuladores Dentales , Análisis del Estrés Dental/instrumentación , Mandíbula/fisiología , Articulación Temporomandibular/fisiología , Fenómenos Biomecánicos , Color , Magnetismo , Cóndilo Mandibular/fisiología , Movimiento , Rango del Movimiento Articular , Rotación , Dimensión Vertical
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