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Int J Biol Macromol ; : 135315, 2024 Sep 03.
Artículo en Inglés | MEDLINE | ID: mdl-39236959

RESUMEN

In this project, a highly efficient catalyst with a remarkable yield of over 97 % was developed for the synthesis of dihydropyrano[2,3-c] pyrazole derivatives. A Gellan Gum-Cellulose hydrogel was prepared using Glutaraldehyde as the cross-linker, which served as the matrix for further modifications. Synthesized graphene oxide was then incorporated into the hydrogel structure using a modified Hummers method, enhancing the catalytic properties of the material. To facilitate the separation and recovery of the catalyst, the resulting structure was magnetized, leading to the formation of a magnetic nanocomposite. Even after undergoing four cycles of catalyst recovery, the GG-Cell hydrogel/GO/Fe3O4 nanocomposite retained 90 % of its initial catalytic activity, highlighting its robustness and stability. Detailed physical and chemical analyses were conducted to gain a comprehensive understanding of the synthesized magnetic catalyst, contributing to the advancement of the field of catalysis and holding great potential for various applications in organic synthesis and related fields.

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