RESUMEN
OBJECTIVE: The aim of this in vitro study was to evaluate the influence of different finishing procedures on the wear behavior of zirconia against natural enamel. METHODS: 64 quadratic specimens (10 mm × 10 mm × 2 mm) were cut from a commercial hipped dental Y-TZP ceramic. Four different groups with 16 specimens each were formed according to the following finishing procedures: PZ (polished), RR (fine-grit diamond), GR (coarse-grit diamond), GZ (glazed). Polished specimens of a leucite-reinforced glass ceramic (Empress CAD) were used as a control (GC). The materials were subjected to the Ivoclar wear method (Willytec chewing simulator, 120,000 cycles, 5kg weight) with 80 natural caries-free cusps of first upper molars as antagonists. Wear was analyzed for both the enamel cusps and test specimens by measurement of the vertical substance loss with a laser scanner. Surface roughness was measured by means of a white-light interferometer. RESULTS: The surface roughness was significantly different among the polished, diamond-finished, and glazed ceramic specimens (ANOVA, post hoc Bonferroni p<0.05). The results of the one-way ANOVA indicated that the finishing technique significantly affected enamel wear (p<0.05). The post hoc test indicated that the specimens finished with the coarse diamond caused significantly higher antagonist wear than the polished ones. Polished zirconia showed the lowest wear of the antagonist enamel, with a mean value of 171.74 (SD = 121.68), and resulted in enamel wear that was not significantly different from that of the glass ceramic control group. No significant linear correlation could be found between pre-testing surface roughness and abrasive wear. SIGNIFICANCE: If zirconia is used without veneering material for crowns and fixed dental prostheses (FDPs), the surface must be well-polished if occlusal adjustments with coarse diamonds are performed. The polishing step reduces the wear of the opposing enamel.
Asunto(s)
Porcelana Dental , Alisadura de la Restauración Dental , Itrio , Circonio , Análisis de Varianza , Esmalte Dental , Pulido Dental , Humanos , Masticación , Microscopía Electrónica de Rastreo , Estadísticas no Paramétricas , Propiedades de SuperficieRESUMEN
OBJECTIVES: The aim of this study was to evaluate the mechanical properties and the subcritical crack growth behavior of a presintered dental Y-TZP (Kavo Everest ZS) and a hot isostatic pressed Y-TZP (Kavo Everest ZH) and to perform life data analysis. METHODS: For each material 150 bending bars were produced. The initial fracture strength was determined in a four-point bending test. The subcritical crack growth parameters n and A were determined in a dynamic fatigue method at four decreasing loading rates from 110MPa/s to 0.11MPa/s in distilled water at 38°C. For each loading rate Weibull statistics were performed and the Weibull moduli m and characteristic strengths σ(0) were calculated. Using these data, strength-fracture probability-life time (SPT) predictions were derived for 1 day, 1 year, 5 years and 10 years, based on a static crack growth mechanism. RESULTS: The "hipped" Y-TZP ceramic exhibited a higher initial strength (σ(c)=1618.18), characteristic strength (σ(0)=837.15) and fracture toughness (K(IC)=4.52MPa/m(1/2)) than the pre-sintered ceramic (σ(c)=1431, σ(0)=745.46 and K(IC)=3.17MPa/m(1/2), respectively). Fatigue parameters, n and A, were 28.5 and 7.97×10(-24) for Everest ZH and 30.15 and 5.47×10(-20) for Everest ZS. The predicted fracture stress at 5% failure probability for a lifetime of 10 years was 259.34MPa for Everest ZH and 263.2MPa for Everest ZS. CONCLUSIONS: Although the "hipped" Y-TZP showed favorable initial mechanical properties, no significant difference could be found in the susceptibility of both ceramics to subcritical crack growth and their long-term strength.