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1.
MethodsX ; 9: 101921, 2022.
Artículo en Inglés | MEDLINE | ID: mdl-36425748

RESUMEN

Participatory mapping is increasingly used to map spatial variation in people's perceptions about ecosystem services. It has growing use in the identification of locations where places perceived to be important converge. Few recommendations have been published to navigate decisions about sampling effort in participatory mapping research when polygon data is collected, although one recommendation is for ≥ 25 participants assuming each participant maps c. 4-5 polygons per ecosystem service. Underlying data informing this recommendation reflects a particular context: collected using postal questionnaires to map a vast spatial area in southern Australia. Although not intended as definitive or suited to all contexts, the 25 participant (or 100-125 polygon) minimum sometimes informs participatory mapping research. Our empirical work, undertaken using face-to-face questionnaires in a small Vietnamese coastal study area, suggests the recommendation may not be appropriate in all contexts. We propose a modified stepwise approach which:•Prioritises spatial agreement (polygon overlap) rather than polygon count and participant numbers to assess data sufficiency•Uses narratives to triangulate outputs generated from participatory mapping data to reduce uncertainty related to low polygon counts.

2.
Nanomaterials (Basel) ; 12(21)2022 Nov 03.
Artículo en Inglés | MEDLINE | ID: mdl-36364663

RESUMEN

The water oxidation of bimetallic Al/Ag nanoparticles has been shown to yield nanoscale structures whose morphology, phase composition and textural characteristics are determined by the synthesis conditions. Flower-like nanoscale structures with silver nanoparticles, with an average size of 17 nm, are formed in water at 60 °C. Under hydrothermal conditions at temperatures of 200 °C and a pressure of 16 MPa, boehmite nanoplatelets with silver nanoparticles, with an average size of 22 nm, are formed. The oxidation of Al/Ag nanoparticles using humid air at 60 °C and 80% relative humidity results in the formation of rod-shaped bayerite nanoparticles and Ag nanoparticles with an average size of 19 nm. The thermal treatment of nanoscale structures obtained at a temperature of 500 °C has been shown to lead to a phase transition into γ-Al2O3, while maintaining the original morphology, and to a decrease in the average size of the silver nanoparticles to 12 nm and their migration to the surface of nanoscale structures. The migration of silver to the nanoparticle surface influences the formation of a double electric layer of particles, and leads to a shift in the pH of the zero-charge point by approximately one, with the nanostructures acquiring pronounced antimicrobial properties.

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