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J Biol Chem ; 282(25): 18286-18293, 2007 Jun 22.
Artículo en Inglés | MEDLINE | ID: mdl-17403673

RESUMEN

Metallo-beta-lactamases (MbetaLs) are zinc-dependent enzymes able to hydrolyze and inactivate most beta-lactam antibiotics. The large diversity of active site structures and metal content among MbetaLs from different sources has limited the design of a pan-MbetaL inhibitor. Here we report the biochemical and biophysical characterization of a novel MbetaL, GOB-18, from a clinical isolate of a Gram-negative opportunistic pathogen, Elizabethkingia meningoseptica. Different spectroscopic techniques, three-dimensional modeling, and mutagenesis experiments, reveal that the Zn(II) ion is bound to Asp120, His121, His263, and a solvent molecule, i.e. in the canonical Zn2 site of dinuclear MbetaLs. Contrasting all other related MbetaLs, GOB-18 is fully active against a broad range of beta-lactam substrates using a single Zn(II) ion in this site. These data further enlarge the structural diversity of MbetaLs.


Asunto(s)
Zinc/química , beta-Lactamasas/fisiología , Sitios de Unión , Clonación Molecular , ADN/química , Flavobacterium/metabolismo , Vectores Genéticos , Hidrólisis , Concentración 50 Inhibidora , Cinética , Modelos Químicos , Datos de Secuencia Molecular , Mutagénesis , Mutagénesis Sitio-Dirigida , Espectrofotometría , beta-Lactamasas/química , beta-Lactamasas/metabolismo
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