RESUMEN
PURPOSE: To evaluate the effect of different concentrations of ethylene-diamine-tetra acetic acid (EDTA) on bond strength (BS) and nanoleakage (NL) of fiber posts bonded into root canals. MATERIALS AND METHODS: Seventy-two single roots were endodontically treated and divided into six groups (n = 12), according to the combination of the following factors: surface treatment (no irrigation [control], 17% EDTA, or 24% EDTA), and composite cement applied with an adhesive used in a self-etch mode (Single Bond Universal/RelyX Ultimate [SB], 3M Oral Care; Ambar Universal/Allcem [AM], FGM). After fiber post cementation, six 1-mm-thick disks were obtained for each root. Push-out bond strength (BS) was evaluated using 8 specimens per group, and the other 4 specimens were used to examine nanoleakage (NL). Data from BS and NL of each adhesive were evaluated by two-way ANOVA (surface treatment vs root region) and Tukey's test (α = 0.05). RESULTS: The application of 17% and 24% EDTA did not influence the bond strengths of either adhesive. In general, the application of 17% and 24% EDTA increased NL values for both adhesives. CONCLUSION: Pre-treatment with different concentrations of EDTA was not able to improve the adhesion of fiber posts into root canals with universal adhesives..
Asunto(s)
Recubrimiento Dental Adhesivo , Técnica de Perno Muñón , Cementos Dentales , Cavidad Pulpar , Dentina , Ácido Edético , Ensayo de Materiales , Cementos de ResinaRESUMEN
Abstract The purpose of this study was to analyze the effect of the application of different concentrations of EDTA on the adhesion of fiber posts to root dentin using self-adhesive resin cements. After endodontic treatment, 78 single roots were randomly divided into six groups (n = 13) according to the combination of the following factors: surface dentin treatment - control (distilled water), 17% EDTA and 24% EDTA; and self-adhesive resin cement - RelyX U200 (RX); and Multilink Speed (ML). After fiber post cementation, six slices were obtained for each root. Ten roots of each group were used for bond strength (BS) and three for microhardness (MH) evaluations. Data obtained from BS and MH tests for each resin cement were subjected to two-way ANOVA (surface treatment vs. root region) and to a post-hoc Tukey's test (α = 0.05). The lowest BS value was observed in the 24% EDTA group for RX cement, whereas the highest values for ML cement were observed for the control group in the middle and apical regions. In the MH test, the lowest value for RX was observed for 24% EDTA in the cervical region, whereas and the highest value for the ML cement was observed in the control group. Regarding both self-adhesive resin cements tested, the application of 24% EDTA was not able to improve the adhesion of fiber posts to root canal.
Asunto(s)
Cementos de Resina , Ensayo de Materiales , Técnica de Perno Muñón , Ácido Edético/farmacología , Cavidad Pulpar , Dentina , VidrioRESUMEN
The purpose of this study was to analyze the effect of the application of different concentrations of EDTA on the adhesion of fiber posts to root dentin using self-adhesive resin cements. After endodontic treatment, 78 single roots were randomly divided into six groups (n = 13) according to the combination of the following factors: surface dentin treatment - control (distilled water), 17% EDTA and 24% EDTA; and self-adhesive resin cement - RelyX U200 (RX); and Multilink Speed (ML). After fiber post cementation, six slices were obtained for each root. Ten roots of each group were used for bond strength (BS) and three for microhardness (MH) evaluations. Data obtained from BS and MH tests for each resin cement were subjected to two-way ANOVA (surface treatment vs. root region) and to a post-hoc Tukey's test (α = 0.05). The lowest BS value was observed in the 24% EDTA group for RX cement, whereas the highest values for ML cement were observed for the control group in the middle and apical regions. In the MH test, the lowest value for RX was observed for 24% EDTA in the cervical region, whereas and the highest value for the ML cement was observed in the control group. Regarding both self-adhesive resin cements tested, the application of 24% EDTA was not able to improve the adhesion of fiber posts to root canal.
Asunto(s)
Cementos de Resina , Cavidad Pulpar , Dentina , Ácido Edético/farmacología , Vidrio , Ensayo de Materiales , Técnica de Perno MuñónRESUMEN
Aim: The roughness and micromorphology of various surface treatments in aged metal-free crowns and the bond strength of these crowns repaired with composite resin (CR) was evaluated in vitro. Methods: A CR core build-up was confectioned in 60 premolars and prepared for metal-free crowns. Prepared teeth were molded with the addition of silicone, and the laboratory ceromer/fiber-reinforced crowns (SR Adoro/Fibrex Lab) were fabricated. Subsequently, the crowns were cemented and artificially aged in a mechanical fatigue device (1.2 X 106 cycles), then divided into 4 groups (n = 15) according to the surface treatment: 1) phosphoric acid etching (PA); 2) PA + silane application; 3) roughening with a diamond bur + PA; and 4) sandblasting with Al2O3 + PA. After the treatments, the crowns (n = 2) were qualitatively analyzed by scanning electron microscope (SEM) and surface roughness (n = 5) was analyzed before and after the surface treatment (Ra parameter). The remaining crowns (n = 8) received standard repair with an adhesive system (Tetric N-Bond) and a nanohybrid CR (Tetric N-Ceram), and the microshear bond strength (SBS) test was performed (0.5 mm/min). Roughness and SBS data were analyzed by one- and two-way ANOVA, respectively, as well as Tukey's post-test (α = 0.05). Results: Sandblasting with Al2O3 + PA resulted in the highest final roughness and SBS values. The lowest results were observed in the PA group, whereas the silane and diamond bur groups showed intermediate values. Conclusion: It may be concluded that indirect ceromer crowns sandblasted with aluminum oxide prior to PA etching promote increased roughness surface and bond strength values
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Propiedades de Superficie , Cerámica , Resinas Compuestas , Resistencia al Corte , Tomografía con Microscopio ElectrónicoRESUMEN
The aim of this study was to compare in vitro the bond strength (BS) between fiberglass posts and flared root canals reinforced with different materials. The roots of 48 premolars were endodontically treated. After one week, the root canals were prepared to simulate an oversized root canal, except for the positive control group (PCG), which was cemented with a prefabricated fiber post (PFP) compatible with the root canal size, simulating an ideal adaptation. The other samples (n=8/group) were used to test alternative restorative techniques for filling root canals: negative control group (NCG [PFP with a smaller diameter than of the root canal]), composite resin group - CRG, bulkfill group - BFG, self-adhesive cement group - SAG, and glass ionomer group - GIG. The posts were cemented and after 1 week, each root was sectioned transversely into six 1-mm thick discs and the push-out test was done to evaluate the BS. Data were analyzed by two-way repeated measures ANOVA and Tukey's tests (α=0.05). The highest BS value was observed for PCG. The NCG and the GIG groups showed the lowest BS values. Root reinforcement with conventional and bulk-fill composite resins showed the highest BS values; however, the bulk-fill resin was the only treatment able to maintain high BS values in all regions of the root canal. The self-adhesive cement showed intermediate results between CRG and GIG. Root reinforcement with bulk-fill composite resin is an effective option for flared root canals before cementation of a prefabricated fiber post.
Asunto(s)
Recubrimiento Dental Adhesivo/métodos , Materiales Dentales/química , Cavidad Pulpar/efectos de los fármacos , Vidrio/química , Técnica de Perno Muñón , Preparación del Conducto Radicular/métodos , Análisis de Varianza , Cavidad Pulpar/anatomía & histología , Fracaso de la Restauración Dental , Humanos , Ensayo de Materiales , Valores de Referencia , Reproducibilidad de los Resultados , Factores de TiempoRESUMEN
Abstract The aim of this study was to compare in vitro the bond strength (BS) between fiberglass posts and flared root canals reinforced with different materials. The roots of 48 premolars were endodontically treated. After one week, the root canals were prepared to simulate an oversized root canal, except for the positive control group (PCG), which was cemented with a prefabricated fiber post (PFP) compatible with the root canal size, simulating an ideal adaptation. The other samples (n=8/group) were used to test alternative restorative techniques for filling root canals: negative control group (NCG [PFP with a smaller diameter than of the root canal]), composite resin group - CRG, bulkfill group - BFG, self-adhesive cement group - SAG, and glass ionomer group - GIG. The posts were cemented and after 1 week, each root was sectioned transversely into six 1-mm thick discs and the push-out test was done to evaluate the BS. Data were analyzed by two-way repeated measures ANOVA and Tukey's tests (α=0.05). The highest BS value was observed for PCG. The NCG and the GIG groups showed the lowest BS values. Root reinforcement with conventional and bulk-fill composite resins showed the highest BS values; however, the bulk-fill resin was the only treatment able to maintain high BS values in all regions of the root canal. The self-adhesive cement showed intermediate results between CRG and GIG. Root reinforcement with bulk-fill composite resin is an effective option for flared root canals before cementation of a prefabricated fiber post.
Asunto(s)
Humanos , Recubrimiento Dental Adhesivo/métodos , Materiales Dentales/química , Cavidad Pulpar/efectos de los fármacos , Vidrio/química , Técnica de Perno Muñón , Preparación del Conducto Radicular/métodos , Análisis de Varianza , Cavidad Pulpar/anatomía & histología , Fracaso de la Restauración Dental , Ensayo de Materiales , Valores de Referencia , Reproducibilidad de los Resultados , Factores de TiempoRESUMEN
PURPOSE: To evaluate the effect of dentin moisture and application mode of universal adhesives on bond strength (BS) and nanoleakage (NL) of fiber posts bonded to root dentin. MATERIALS AND METHODS: The roots of 96 extracted human canines were treated endodontically, and the fiber posts were cemented according to the combination of the following factors: dentin moisture (dry and wet), cementation system [Single Bond Universal/RelyX ARC (SBU) and Prime&Bond elect/Enforce (PBE)], and adhesive application [active (A) and passive (P)] in accordance with the manufacturer's instructions. After one week, the specimens were transversely sectioned into six 1-mm-thick disks. From each group, 8 specimens were subjected to the push-out BS test and the other 4 specimens underwent NL analysis. For both tests, the data were subjected to 3-way repeated measures ANOVA and Tukey's tests (α = 0.05). RESULTS: For BS and NL, the cross-product interaction of all factors was significant (p < 0.05). Lower BS was observed under P application independent of the dentin moisture; for A application, SBU showed higher BS than did PBE in both moisture conditions. Nanoleakage was present in all groups and ranged from 22.9% to 36%. CONCLUSION: The active application of universal adhesives improves the adhesion in fiber post cementation, independent of dentin moisture condition.